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Pregled bibliografske jedinice broj: 962183

HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage

Ivešić, Martina; Kuharić, Željka; Pavlek, Željka; Jakopović, Željko; Čanak, Iva; Frece, Jadranka; Markov, Ksenija; Bošnir, Jasna
HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage // Toxicology Letters
Bruxelles, Belgija, 2018. str. 147-148 doi:10.1016/j.toxlet.2018.06.742 (poster, međunarodna recenzija, sažetak, znanstveni)

CROSBI ID: 962183 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage

Autori
Ivešić, Martina ; Kuharić, Željka ; Pavlek, Željka ; Jakopović, Željko ; Čanak, Iva ; Frece, Jadranka ; Markov, Ksenija ; Bošnir, Jasna

Vrsta, podvrsta i kategorija rada
Sažeci sa skupova, sažetak, znanstveni

Izvornik
Toxicology Letters / - , 2018, 147-148

Skup
54th Congress of the European Societies of Toxicology: Toxicology out of the Box (EUROTOX 2018)

Mjesto i datum
Bruxelles, Belgija, 02.09.2018. - 05.09.2018

Vrsta sudjelovanja
Poster

Vrsta recenzije
Međunarodna recenzija

Ključne riječi
Aflatoxin M1, Food safety, Mycotoxin-binding agents, HPLC-FLD, LC-MS/MS

Sažetak
The toxicity of aflatoxin M1 (AFM1) has a high importance for the food quality and possible entrance in human body. Mycotoxin-binding agents (MBA) could be used for fixation of AFM1 to minimise exposure through dairy products. The purpose of this study was to determine unbounded amounts of AFM1 after adding of lactic acid bacteria (LAB) and β-glucan (cellular yeast components) added firstly for binding then removing aflatoxin AFM1 from milk. LAB were isolated from fresh cow's milk and traditional dairy products such as: fresh cow cheese and cream. All milk samples used in the experiment were first analysed and verified for AFM1 contamination free, than spiked with known amount of AFM1. Membrane filtration method and Centricon Plus-70, a MWCO 100 kDa were selected for removal of resulting biofixator-AFM1 complex from milk.The concentration of AFM1 residues in the samples were determined by high performance liquid chromatography using a fluorescent detector (HPLC-FLD). Previously obtained values were confirmed by high performance liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS). Before HPLC or LC-MS/MS analysis the samples were purified on immunoaffinity columns. Both methods were fully validated by determination of following validation parameters: selectivity, linearity, precision, accuracy, recovery, limits of detection and quantification. Validation data proved that both methods are suitable for determination of AFM1 residues in milk. Obtained results of AFM1 after removed biofixator-AFM1 complex from milk shown very good correlation between both methods.

Izvorni jezik
Engleski

Znanstvena područja
Biotehnologija, Prehrambena tehnologija



POVEZANOST RADA

Ustanove:
Prehrambeno-biotehnološki fakultet, Zagreb

Profili:

Avatar Url Željka Pavlek (autor)

Avatar Url Jadranka Frece (autor)

Avatar Url Željko Jakopović (autor)

Avatar Url Martina Ivešić (autor)

Avatar Url Jasna Bošnir (autor)

Avatar Url Iva Čanak (autor)

Avatar Url Ksenija Markov (autor)

Poveznice na cjeloviti tekst rada:

doi www.sciencedirect.com

Citiraj ovu publikaciju:

Ivešić, Martina; Kuharić, Željka; Pavlek, Željka; Jakopović, Željko; Čanak, Iva; Frece, Jadranka; Markov, Ksenija; Bošnir, Jasna
HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage // Toxicology Letters
Bruxelles, Belgija, 2018. str. 147-148 doi:10.1016/j.toxlet.2018.06.742 (poster, međunarodna recenzija, sažetak, znanstveni)
Ivešić, M., Kuharić, Ž., Pavlek, Ž., Jakopović, Ž., Čanak, I., Frece, J., Markov, K. & Bošnir, J. (2018) HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage. U: Toxicology Letters doi:10.1016/j.toxlet.2018.06.742.
@article{article, author = {Ive\v{s}i\'{c}, Martina and Kuhari\'{c}, \v{Z}eljka and Pavlek, \v{Z}eljka and Jakopovi\'{c}, \v{Z}eljko and \v{C}anak, Iva and Frece, Jadranka and Markov, Ksenija and Bo\v{s}nir, Jasna}, year = {2018}, pages = {147-148}, DOI = {10.1016/j.toxlet.2018.06.742}, keywords = {Aflatoxin M1, Food safety, Mycotoxin-binding agents, HPLC-FLD, LC-MS/MS}, doi = {10.1016/j.toxlet.2018.06.742}, title = {HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage}, keyword = {Aflatoxin M1, Food safety, Mycotoxin-binding agents, HPLC-FLD, LC-MS/MS}, publisherplace = {Bruxelles, Belgija} }
@article{article, author = {Ive\v{s}i\'{c}, Martina and Kuhari\'{c}, \v{Z}eljka and Pavlek, \v{Z}eljka and Jakopovi\'{c}, \v{Z}eljko and \v{C}anak, Iva and Frece, Jadranka and Markov, Ksenija and Bo\v{s}nir, Jasna}, year = {2018}, pages = {147-148}, DOI = {10.1016/j.toxlet.2018.06.742}, keywords = {Aflatoxin M1, Food safety, Mycotoxin-binding agents, HPLC-FLD, LC-MS/MS}, doi = {10.1016/j.toxlet.2018.06.742}, title = {HPLC-FLD and LC-MS/MS determination of Aflatoxin M1 from milk after biofixators usage}, keyword = {Aflatoxin M1, Food safety, Mycotoxin-binding agents, HPLC-FLD, LC-MS/MS}, publisherplace = {Bruxelles, Belgija} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE

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