Pregled bibliografske jedinice broj: 860345
Eco-friendly rapid synthesis of 3-substituted- 2- thioxo-2, 3-dihydroquinazolin-4(1H)-ones in choline chloride based deep eutectic solvent
Eco-friendly rapid synthesis of 3-substituted- 2- thioxo-2, 3-dihydroquinazolin-4(1H)-ones in choline chloride based deep eutectic solvent // Synthetic communications, 47 (2017), 11; 1040-1045 doi:10.1080/00397911.2017.1291815 (međunarodna recenzija, članak, znanstveni)
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Naslov
Eco-friendly rapid synthesis of 3-substituted- 2- thioxo-2, 3-dihydroquinazolin-4(1H)-ones in choline chloride based deep eutectic solvent
Autori
Molnar, Maja ; Klenkar, Jelena ; Tarnai, Tena
Izvornik
Synthetic communications (0039-7911) 47
(2017), 11;
1040-1045
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
deep eutectic solvents ; 2-thioxo-2, 3-dihydroquinazolin-4(1H)-ones ; anthranilic acid ; 5-iodoanthranilic acid ; isothiocyanate
Sažetak
A series of 3-substituted-2-thioxo-2, 3- dihydroquinazolin-4(1H)-ones and 6-iodo-3- substituted-2-thioxo-2, 3-dihydroquinazolin- 4(1H)-ones were synthesized in choline chloride/urea deep eutectic solvent. Substituted 2-mercapto-4(3H)-quinazolinones were synthesized from anthranilic acid or 5- iodoanthranilic acid and appropriate isothiocyanates in good to excellent yields. Isolation of final product was easy and required no further purification. Synthesis of these compounds was rapid, selective and catalyst free, while preparation of deep eutectic solvent was easy, components are readily available, cheap and environmentally friendly.
Izvorni jezik
Engleski
Znanstvena područja
Kemija, Prehrambena tehnologija
POVEZANOST RADA
Ustanove:
Prehrambeno-tehnološki fakultet, Osijek
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- Arts & Humanities Citation Index (A&HCI)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus