Optimization condition for thin-layer identification of bronzes after anodic sampling

Ašperger, Danijela; Ćurković, Lidija; Horvat, Alka J.M.; Kaštelan-Macan, Marija

doi:10.1556/JPC.27.2014.2.2

Pregled bibliografske jedinice broj: 653468

Optimization condition for thin-layer identification of bronzes after anodic sampling

Ašperger, Danijela; Ćurković, Lidija; Horvat, Alka J.M.; Kaštelan-Macan, Marija

Optimization condition for thin-layer identification of bronzes after anodic sampling // JPC. Journal of planar chromatography, modern TLC, 27 (2014), 2; 84-87 doi:10.1556/JPC.27.2014.2.2 (međunarodna recenzija, članak, znanstveni)

CROSBI ID: 653468 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Optimization condition for thin-layer identification of bronzes after anodic sampling

Autori
Ašperger, Danijela ; Ćurković, Lidija ; Horvat, Alka J.M. ; Kaštelan-Macan, Marija

Izvornik
JPC. Journal of planar chromatography, modern TLC (0933-4173) 27 (2014), 2; 84-87

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Cu-alloy; Anodic sampling; Identification of metal ions; Thin-layer chromatography - TLC

Sažetak
Qualitative identification of Cu, Sn, Pb, Ni, and Fe in Cu-alloys is presented. The method involves anodic sampling of alloys, separation and identification by thin-layer chromatography (TLC). The powerful desktop-computer tool makes it easy to optimize ternary solvent mixtures. Optimization was performed graphically by means of RSi1 as a selected separation criterion. Mobile phase composition for optimal separation was determined as MeOH:HCl:H2O (60+35+5, v/v). The method was applied to Persian helmet as real sample.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Strojarstvo

POVEZANOST RADA

Ustanove:
Fakultet strojarstva i brodogradnje, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb

Profili:

Lidija Ćurković (autor)