Naslov
A fast method for multi-metal determination in the soil samples by high-resolution inductively-coupled plasma-mass spectrometry (HR-ICP-MS)

Autori
Roje, Vibor

Izvornik
Chemical speciation and bioavailability (0954-2299) 22 (2010), 2; 135-139

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, kratko priopcenje, znanstveni

Ključne riječi
inductively coupled plasma mass spectrometry ; microwave digestion ; recovery ; soil ; trace elements

Sažetak
Methods for multi-elemental quantitative analysis of soil samples by high-resolution inductively-coupled plasma-mass spectrometry (HR– ICP–MS) with preceding one-step wet digestion in a high-pressure microwave system have been developed. The application of aqua regia as a reagent for wet digestion using a high-pressure microwave digestion system, followed by determination using HR–ICP–MS, allows an accurate, simultaneous determination of a large number of heavy metals and metalloids that are considered as potentially hazardous for the environment and health. The values of the concentrations of the elements in the analysed certified reference material (CRM) that have been obtained in this study can be used as indicative values where this CRM is used as a control for the quality of the measurements.

Izvorni jezik
Engleski

Znanstvena područja
Kemija

POVEZANOST RADA