Pregled bibliografske jedinice broj: 475413
Multi-elemental analysis of marine sediment reference material MESS-3: one-step microwave digestion and determination by high resolution inductively coupled plasma-mass spectrometry (HR-ICP-MS)
Multi-elemental analysis of marine sediment reference material MESS-3: one-step microwave digestion and determination by high resolution inductively coupled plasma-mass spectrometry (HR-ICP-MS) // Chemical papers, 64 (2010), 4; 409-414 doi:10.2478/s11696-010-0022-x (međunarodna recenzija, članak, znanstveni)
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Naslov
Multi-elemental analysis of marine sediment reference material MESS-3: one-step microwave digestion and determination by high resolution inductively coupled plasma-mass spectrometry (HR-ICP-MS)
Autori
Roje, Vibor
Izvornik
Chemical papers (0366-6352) 64
(2010), 4;
409-414
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
rapid elemental analysis ; inductively coupled plasma mass spectrometry ; microwave digestion ; marine sediment ; trace elements
Sažetak
Single-step microwave digestion methods using four different acidic dissolving reagents were investigated with the main objective to obtain a simple, rapid method for multi-elemental analysis of marine sediment samples by high resolution inductively coupled plasma-mass spectrometry (HR-ICP-MS), especially for environmental studies. Closed-vessels microwave digestion procedures were carried out using the reagents as follows: HNO3, mixture of HNO3–HCl (ϕr = 9 : 1), aqua regia, and mixture of HNO3–HCl–HF (ϕr = 8 : 1 : 1). The elements analyzed were: Al, As, Ba, Be, Bi, Cd, Co, Cr, Cu, Fe, K, Li, Mn, Mo, Na, Ni, Pb, Sb, Sn, Sr, Ti, Tl, V, and Zn. Good recoveries were established for many of the metals analyzed even when only nitric acid was employed. However, for a good recovery of Sb and Tl, aqua regia should be employed.
Izvorni jezik
Engleski
Znanstvena područja
Kemija
POVEZANOST RADA
Projekti:
098-0982934-2713 - Radionuklidi i elementi u tragovima u okolišnim sustavima (Barišić, Delko, MZOS ) ( CroRIS)
Ustanove:
Institut "Ruđer Bošković", Zagreb
Profili:
Vibor Roje
(autor)
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus
Uključenost u ostale bibliografske baze podataka::
- Analytical Abstracts
- Chemical Engineering and Biotechnology Abstracts
- Abstract Bulletin of the Institute of Paper Chemistry
- Annual Scientific Congress Abstracts
- Biological Abstracts
- CADSCAN
- Chemical Abstracts
- ChemInform
- Chemistry Citation Index
- CISA
- Index to Scientific Reviews
- LeadScan
- Mass Spectrometry Bulletin
- Materials Science
