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Pregled bibliografske jedinice broj: 396078

Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation

Vrdoljak, Višnja; Pisk, Jana; Prugovečki, Biserka; Matković-Čalogović, Dubravka
Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation // Inorganica chimica acta, 362 (2009), 11; 4059-4064 doi:10.1016/j.ica.2009.05.057 (međunarodna recenzija, članak, znanstveni)

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Naslov
Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation

Autori
Vrdoljak, Višnja ; Pisk, Jana ; Prugovečki, Biserka ; Matković-Čalogović, Dubravka

Izvornik
Inorganica chimica acta (0020-1693) 362 (2009), 11; 4059-4064

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Molybdenum(VI) complexes ; molybdenum(V) complexes ; thiosemicarbazone ; pyridoxal ; crystal structure

Sažetak
New molybdenum complexes were prepared by the reaction of [MoVIO2(acac)2] or (NH4)2[MoVOCl5] with different N-substituted pyridoxal thiosemicarbazone ligands (H2L1 = pyridoxal 4- phenylthiosemicarbazone ; H2L2 = pyridoxal 4- methylthiosemicarbazone, H2L3 = pyridoxal thiosemicarbazone). The investigation of monomeric [MoO2L1(CH3OH)] or polymeric [MoO2L1-3] molybdenum(VI) complexes revealed that molybdenum is coordinated with a tridentate doubly- deprotonated ligand. In the oxomolybdenum(V) complexes [MoOCl2(HL1-3)] the pyridoxal thiosemicarbazonato ligands are tridentate mono- deprotonated. Crystal and molecular structures of molybdenum(VI) [MoO2L1(CH3OH)]∙ CH3OH, and molybdenum(V) complexes [MoOCl2(HL1)]∙ C2H5OH, as well as of the pyridoxal thiosemicarbazone ligand methanol solvate H2L3∙ MeOH, were determined by the single crystal X-ray diffraction method.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
MZOS-119-1191342-1082 - Novi kompleksni spojevi i materijali-kemijski i biološki katalizatori (Cindrić, Marina, MZOS ) ( CroRIS)
MZOS-119-1193079-1084 - Strukturno istraživanje bioloških makromolekula metodom rentgenske difrakcije (Matković-Čalogović, Dubravka, MZOS ) ( CroRIS)

Ustanove:
Prirodoslovno-matematički fakultet, Zagreb

Profili:

Avatar Url Višnja Vrdoljak (autor)

Avatar Url Dubravka Matković-Čalogović (autor)

Avatar Url Jana Pisk (autor)

Avatar Url Biserka Prugovečki (autor)

Poveznice na cjeloviti tekst rada:

doi www.sciencedirect.com

Citiraj ovu publikaciju:

Vrdoljak, Višnja; Pisk, Jana; Prugovečki, Biserka; Matković-Čalogović, Dubravka
Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation // Inorganica chimica acta, 362 (2009), 11; 4059-4064 doi:10.1016/j.ica.2009.05.057 (međunarodna recenzija, članak, znanstveni)
Vrdoljak, V., Pisk, J., Prugovečki, B. & Matković-Čalogović, D. (2009) Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation. Inorganica chimica acta, 362 (11), 4059-4064 doi:10.1016/j.ica.2009.05.057.
@article{article, author = {Vrdoljak, Vi\v{s}nja and Pisk, Jana and Prugove\v{c}ki, Biserka and Matkovi\'{c}-\v{C}alogovi\'{c}, Dubravka}, year = {2009}, pages = {4059-4064}, DOI = {10.1016/j.ica.2009.05.057}, keywords = {Molybdenum(VI) complexes, molybdenum(V) complexes, thiosemicarbazone, pyridoxal, crystal structure}, journal = {Inorganica chimica acta}, doi = {10.1016/j.ica.2009.05.057}, volume = {362}, number = {11}, issn = {0020-1693}, title = {Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation}, keyword = {Molybdenum(VI) complexes, molybdenum(V) complexes, thiosemicarbazone, pyridoxal, crystal structure} }
@article{article, author = {Vrdoljak, Vi\v{s}nja and Pisk, Jana and Prugove\v{c}ki, Biserka and Matkovi\'{c}-\v{C}alogovi\'{c}, Dubravka}, year = {2009}, pages = {4059-4064}, DOI = {10.1016/j.ica.2009.05.057}, keywords = {Molybdenum(VI) complexes, molybdenum(V) complexes, thiosemicarbazone, pyridoxal, crystal structure}, journal = {Inorganica chimica acta}, doi = {10.1016/j.ica.2009.05.057}, volume = {362}, number = {11}, issn = {0020-1693}, title = {Novel Dioxomolybdenum(VI) and Oxomolybdenum(V) Complexes with Pyridoxal Thiosemicarbazone Ligands: Synthesis and Structural Characterisation}, keyword = {Molybdenum(VI) complexes, molybdenum(V) complexes, thiosemicarbazone, pyridoxal, crystal structure} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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