Pretraga

Pretražite po imenu i prezimenu autora, mentora, urednika, prevoditelja

Napredna pretraga

Pregled bibliografske jedinice broj: 368356

Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone

Gazivoda, Tatjana; Raić-Malić, Silvana; Hergold-Brundić, Antonija; Cetina, Mario
Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone // Molecules, 13 (2008), 11; 2786-2795 doi:10.3390/molecules13112786 (međunarodna recenzija, članak, znanstveni)

CROSBI ID: 368356 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone

Autori
Gazivoda, Tatjana ; Raić-Malić, Silvana ; Hergold-Brundić, Antonija ; Cetina, Mario

Izvornik
Molecules (1420-3049) 13 (2008), 11; 2786-2795

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
5-(2-haloethyl)pyrimidine ; synthesis ; X-ray crystal structure ; hydrogen bonds

Sažetak
Three novel 5-(2-haloethyl)pyrimidine derivatives were synthesized and characterized by 1H-NMR, 13C-NMR, MS, IR spectra and elemental analysis. Iodine and chlorine atoms in the C-5 side chain were introduced by reaction of 5-(2-hydroxyethyl)pyrimidine with hydroiodic acid and phosphoryl chloride, respectively. The structure of the intermediate  -(1-carbamyliminomethylene)- -butyrolactone was determined by X-ray crystal structure analysis. The molecule deviates very slightly from planarity. Three N H• • • O hydrogen bonds link the molecules into one-dimensional chains of edge-fused rings.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
MZOS-125-0982464-2925 - Razvoj i primjena novih molekula u pozitron-emisijskoj tomografiji (PET) (Raić-Malić, Silvana, MZOS ) ( CroRIS)

Ustanove:
Tekstilno-tehnološki fakultet, Zagreb,
Prirodoslovno-matematički fakultet, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb

Profili:

Avatar Url Silvana Raić-Malić (autor)

Avatar Url Mario Cetina (autor)

Avatar Url Antonija Hergold-Brundić (autor)

Avatar Url Tatjana Gazivoda Kraljević (autor)

Poveznice na cjeloviti tekst rada:

doi doi.org www.mdpi.com

Citiraj ovu publikaciju:

Gazivoda, Tatjana; Raić-Malić, Silvana; Hergold-Brundić, Antonija; Cetina, Mario
Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone // Molecules, 13 (2008), 11; 2786-2795 doi:10.3390/molecules13112786 (međunarodna recenzija, članak, znanstveni)
Gazivoda, T., Raić-Malić, S., Hergold-Brundić, A. & Cetina, M. (2008) Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone. Molecules, 13 (11), 2786-2795 doi:10.3390/molecules13112786.
@article{article, author = {Gazivoda, Tatjana and Rai\'{c}-Mali\'{c}, Silvana and Hergold-Brundi\'{c}, Antonija and Cetina, Mario}, year = {2008}, pages = {2786-2795}, DOI = {10.3390/molecules13112786}, keywords = {5-(2-haloethyl)pyrimidine, synthesis, X-ray crystal structure, hydrogen bonds}, journal = {Molecules}, doi = {10.3390/molecules13112786}, volume = {13}, number = {11}, issn = {1420-3049}, title = {Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone}, keyword = {5-(2-haloethyl)pyrimidine, synthesis, X-ray crystal structure, hydrogen bonds} }
@article{article, author = {Gazivoda, Tatjana and Rai\'{c}-Mali\'{c}, Silvana and Hergold-Brundi\'{c}, Antonija and Cetina, Mario}, year = {2008}, pages = {2786-2795}, DOI = {10.3390/molecules13112786}, keywords = {5-(2-haloethyl)pyrimidine, synthesis, X-ray crystal structure, hydrogen bonds}, journal = {Molecules}, doi = {10.3390/molecules13112786}, volume = {13}, number = {11}, issn = {1420-3049}, title = {Synthesis and structural characterization of the 5-(2-haloethyl)pyrimidines – hydrogen-bonded chains in α-(1-carbamyliminomethylene)-γ-butyrolactone}, keyword = {5-(2-haloethyl)pyrimidine, synthesis, X-ray crystal structure, hydrogen bonds} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE

Citati:

    Altmetrijski pokazatelji:


    Podijeli:





    Contrast
    Increase Font
    Decrease Font
    Dyslexic Font
    CROSBI koristi kolačiće (cookies) kako bi poboljšao funkcionalnost stranice.