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Pregled bibliografske jedinice broj: 304981

Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state.

Kukovec, Boris-Marko; Popović, Zora; Pavlović, Gordana; Rajić Linarić, Maša
Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state. // Journal of Molecular Structure, 882 (2008), 47-55 (međunarodna recenzija, članak, znanstveni)

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Naslov
Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state.

Autori
Kukovec, Boris-Marko ; Popović, Zora ; Pavlović, Gordana ; Rajić Linarić, Maša

Izvornik
Journal of Molecular Structure (0022-2860) 882 (2008); 47-55

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Cobalt(II) complexes; 6-hydroxypicolinic acid; 2-hydroxynicotinic acid; Polymorphism; Crystal structures; IR-spectra; TGA/DSC measurements

Sažetak
Cobalt(II) complexes of 6-hydroxypicolinic acid (6-OHpicH), namely [Co(6-OHpic)2(H2O)2] (1) and [Co(6-OHpic)2(4-pic)2]∙ 4-pic (2), and of 2-hydroxynicotinic acid (2-OHnicH), [Co(2-OHnic)2(H2O)2] (3) were prepared. The crystal structures of free 6-hydroxypicolinic acid monohydrate [6-OHpicH]• H2O (4), and the novel polymorph of 2-hydroxynicotinic acid [2-OHnicH] (5) and complex 2 were determined by X-ray crystal structure analysis. All compounds were characterized by IR-spectroscopy and thermal methods and data are in agreement with the structure analysis. It was established that 4 and 5 exist in solid state in keto-tautomeric form. For 2, structure analysis revealed N, O-chelating mode of 6-hydroxypicolinic acid.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
119-1193079-1332 - Kemija metalnih kompleksa u reakcijama od biološkog značaja i novim materijalima (Popović, Zora, MZOS ) ( CroRIS)
192-1252971-1982 - Istraživanje procesa starenja i predikcija životnog vijeka materijala (Sućeska, Muhamed, MZOS ) ( CroRIS)

Ustanove:
Prirodoslovno-matematički fakultet, Zagreb

Profili:

Avatar Url Zora Popović (autor)

Avatar Url Maša Rajić Linarić (autor)

Avatar Url Gordana Pavlović (autor)

Avatar Url Boris-Marko Kukovec (autor)

Citiraj ovu publikaciju:

Kukovec, Boris-Marko; Popović, Zora; Pavlović, Gordana; Rajić Linarić, Maša
Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state. // Journal of Molecular Structure, 882 (2008), 47-55 (međunarodna recenzija, članak, znanstveni)
Kukovec, B., Popović, Z., Pavlović, G. & Rajić Linarić, M. (2008) Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state.. Journal of Molecular Structure, 882, 47-55.
@article{article, author = {Kukovec, Boris-Marko and Popovi\'{c}, Zora and Pavlovi\'{c}, Gordana and Raji\'{c} Linari\'{c}, Ma\v{s}a}, year = {2008}, pages = {47-55}, keywords = {Cobalt(II) complexes, 6-hydroxypicolinic acid, 2-hydroxynicotinic acid, Polymorphism, Crystal structures, IR-spectra, TGA/DSC measurements}, journal = {Journal of Molecular Structure}, volume = {882}, issn = {0022-2860}, title = {Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state.}, keyword = {Cobalt(II) complexes, 6-hydroxypicolinic acid, 2-hydroxynicotinic acid, Polymorphism, Crystal structures, IR-spectra, TGA/DSC measurements} }
@article{article, author = {Kukovec, Boris-Marko and Popovi\'{c}, Zora and Pavlovi\'{c}, Gordana and Raji\'{c} Linari\'{c}, Ma\v{s}a}, year = {2008}, pages = {47-55}, keywords = {Cobalt(II) complexes, 6-hydroxypicolinic acid, 2-hydroxynicotinic acid, Polymorphism, Crystal structures, IR-spectra, TGA/DSC measurements}, journal = {Journal of Molecular Structure}, volume = {882}, issn = {0022-2860}, title = {Synthesis and structure of cobalt(II) complexes with hydroxyl derivatives of pyridinecarboxylic acids. Conformation analysis of ligands in the solid state.}, keyword = {Cobalt(II) complexes, 6-hydroxypicolinic acid, 2-hydroxynicotinic acid, Polymorphism, Crystal structures, IR-spectra, TGA/DSC measurements} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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