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Pregled bibliografske jedinice broj: 155967

Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography

Rezić, Iva; Horvat, Alka J.M.; Babić, Sandra; Kaštelan-Macan, Marija
Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography // Ultrasonics sonochemistry, 12 (2005), 6; 477-481 doi:10.1016/j.ultsonch.2004.07.004 (međunarodna recenzija, članak, znanstveni)

CROSBI ID: 155967 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography

Autori
Rezić, Iva ; Horvat, Alka J.M. ; Babić, Sandra ; Kaštelan-Macan, Marija

Izvornik
Ultrasonics sonochemistry (1350-4177) 12 (2005), 6; 477-481

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
ultrasonic solvent extraction ; thin layer chromatography ; pesticides

Sažetak
A rapid method for quantitative determination of atrazine and simazine in honey samples was investigated. The procedure was based on the extraction of pesticides by sonication with benzene:water = 1:1 (v/v) mixture, thin-layer chromatographic separation and quantification by CAMAG Video Documentation system in conjunction with the Reprostar 3. The extraction procedure was optimized with regard to the amount of solvent, duration of sonication and the number of extraction steps. The apparent recovery of pesticides from honey was 92.3 +/- 2.4 for atrazine and 94.2 +/- 2.8 for simazine, when they were extracted in three steps for 20 min using 20 ml of solvent. Ultrasonic solvent extraction was compared with traditional shake-flask extraction method.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Tekstilna tehnologija



POVEZANOST RADA

Projekti:
0117012
0125055

Ustanove:
Tekstilno-tehnološki fakultet, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb

Profili:

Avatar Url Sandra Babić (autor)

Avatar Url Iva Rezić (autor)

Avatar Url Alka Horvat (autor)

Avatar Url Marija Kaštelan-Macan (autor)

Poveznice na cjeloviti tekst rada:

doi dx.doi.org www.sciencedirect.com

Citiraj ovu publikaciju:

Rezić, Iva; Horvat, Alka J.M.; Babić, Sandra; Kaštelan-Macan, Marija
Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography // Ultrasonics sonochemistry, 12 (2005), 6; 477-481 doi:10.1016/j.ultsonch.2004.07.004 (međunarodna recenzija, članak, znanstveni)
Rezić, I., Horvat, A., Babić, S. & Kaštelan-Macan, M. (2005) Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography. Ultrasonics sonochemistry, 12 (6), 477-481 doi:10.1016/j.ultsonch.2004.07.004.
@article{article, author = {Rezi\'{c}, Iva and Horvat, Alka J.M. and Babi\'{c}, Sandra and Ka\v{s}telan-Macan, Marija}, year = {2005}, pages = {477-481}, DOI = {10.1016/j.ultsonch.2004.07.004}, keywords = {ultrasonic solvent extraction, thin layer chromatography, pesticides}, journal = {Ultrasonics sonochemistry}, doi = {10.1016/j.ultsonch.2004.07.004}, volume = {12}, number = {6}, issn = {1350-4177}, title = {Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography}, keyword = {ultrasonic solvent extraction, thin layer chromatography, pesticides} }
@article{article, author = {Rezi\'{c}, Iva and Horvat, Alka J.M. and Babi\'{c}, Sandra and Ka\v{s}telan-Macan, Marija}, year = {2005}, pages = {477-481}, DOI = {10.1016/j.ultsonch.2004.07.004}, keywords = {ultrasonic solvent extraction, thin layer chromatography, pesticides}, journal = {Ultrasonics sonochemistry}, doi = {10.1016/j.ultsonch.2004.07.004}, volume = {12}, number = {6}, issn = {1350-4177}, title = {Determination of pesticides in honey by ultrasonic solvent extraction and thin-layer chromatography}, keyword = {ultrasonic solvent extraction, thin layer chromatography, pesticides} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE

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  • CA Search (Chemical Abstracts)

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