Pregled bibliografske jedinice broj: 1216272
Real-Time in Situ Monitoring of Particle and Structure Evolution in the Mechanochemical Synthesis of UiO-66 Metal–Organic Frameworks
Real-Time in Situ Monitoring of Particle and Structure Evolution in the Mechanochemical Synthesis of UiO-66 Metal–Organic Frameworks // Crystal growth & design, 20 (2020), 1; 49-54 doi:10.1021/acs.cgd.9b01477 (međunarodna recenzija, članak, znanstveni)
CROSBI ID: 1216272 Za ispravke kontaktirajte CROSBI podršku putem web obrasca
Naslov
Real-Time in Situ Monitoring of Particle and
Structure Evolution in the Mechanochemical
Synthesis of UiO-66 Metal–Organic Frameworks
Autori
Germann, Luzia S. ; Katsenis, Athanassios D. ; Huskić, Igor ; Julien, Patrick A. ; Užarević, Krunoslav ; Etter, Martin ; Farha, Omar K. ; Friščić, Tomislav ; Dinnebier, Robert E.
Izvornik
Crystal growth & design (1528-7483) 20
(2020), 1;
49-54
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
Mechanochemistry ; zirconium MOFs ; UiO-66 ; particle size ; in situ
Sažetak
While in situ synchrotron X-ray powder diffraction has revolutionized mechanistic studies of mechanochemistry and inspired the development of other real-time monitoring approaches, the full potential of such data remains unexploited, with most applications addressing only reaction kinetics. Focusing on UiO-type metal–organic frameworks (MOFs) as models, we now show how in- depth analysis of real-time diffraction data can provide insight into the evolution of both crystallographic structure and crystallite size, including the direct relation to the particle size of mechanochemically formed MOFs.
Izvorni jezik
Engleski
Znanstvena područja
Kemija
POVEZANOST RADA
Projekti:
HRZZ-PZS-2019-02-4129 - Mehanokemijske i bezotopinske strategije za sintezu funkcionalnih poroznih materijala s naprednim fizičko-kemijskim i katalitičkim svojstvima (MECHADVANCE) (Užarević, Krunoslav, HRZZ - 2019-02) ( CroRIS)
Ustanove:
Institut "Ruđer Bošković", Zagreb
Profili:
Krunoslav Užarević
(autor)
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus