Pregled bibliografske jedinice broj: 891163
In-situ Raman Spectroscopic Monitoring of Ball Milling Preparations of Amidoboranes
In-situ Raman Spectroscopic Monitoring of Ball Milling Preparations of Amidoboranes // INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying : Program and Abstracts / Šepelák, Vladimír (ur.).
Košice, 2017. str. 91-91 (poster, nije recenziran, sažetak, ostalo)
CROSBI ID: 891163 Za ispravke kontaktirajte CROSBI podršku putem web obrasca
Naslov
In-situ Raman Spectroscopic Monitoring of Ball Milling Preparations of Amidoboranes
Autori
Biliškov, Nikola ; Halasz, Ivan ; Užarević, Krunoslav ; Grbović Novaković, Jasmina ; Milanović, Igor ; Lukin, Stipe ; Milošević, Sanja ; Borgschulte, Andreas ; Callini, Elsa
Vrsta, podvrsta i kategorija rada
Sažeci sa skupova, sažetak, ostalo
Izvornik
INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying : Program and Abstracts
/ Šepelák, Vladimír - Košice, 2017, 91-91
Skup
INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying
Mjesto i datum
Košice, Slovačka, 03.09.2017. - 07.09.2017
Vrsta sudjelovanja
Poster
Vrsta recenzije
Nije recenziran
Ključne riječi
hydrogen storage ; amidoborane ; Raman spectroscopy
Sažetak
Recently, a few techniques that allow in-situ monitoring of ball milling reaction in real time are developed and well established.[1] For the first time, we applied one of these techniques, Raman spectroscopy, in order to follow up the mechanochemical synthesis of materials for solid-state hydrogen storage. Specifically, a series of single- and bimetallic amidoboranes of MAB, MAB·AB and M2MgAB4 (M = Li, Na ; AB = NH3BH3) composition were prepared and thoroughly characterized. A detailed analysis of spectral data revealed that in all cases a two step mechanism takes place through MAB·AB adducts as a key intermediate phase.
Izvorni jezik
Engleski
Znanstvena područja
Kemija
POVEZANOST RADA
Projekti:
HRZZ-PKP-2016-06-4480 - Novi materijali za pohranu energije (NEWMATENG) (Halasz, Ivan, HRZZ - 2016-06) ( CroRIS)
Ustanove:
Institut "Ruđer Bošković", Zagreb