Pregled bibliografske jedinice broj: 75708
Synthesis of acicular a-FeOOH particles at a very high pH
Synthesis of acicular a-FeOOH particles at a very high pH // Materials letters, 54 (2002), 2-3; 108-113 doi:10.1016/S0167-577X(01)00546-8 (međunarodna recenzija, članak, znanstveni)
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Naslov
Synthesis of acicular a-FeOOH particles at a very high pH
Autori
Krehula, Stjepko ; Popović, Stanko ; Musić, Svetozar
Izvornik
Materials letters (0167-577X) 54
(2002), 2-3;
108-113
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
goethite ; tetramethylammonium hydroxide ; acicular particles ; XRD ; FT-IR ; TEM
Sažetak
The acicular α-FeOOH particles were synthesized from FeCl3 solutions at a very high pH using tetramethylammonium hydroxide as a precipitating agent. Samples were characterized by X-ray powder diffraction, FT-IR spectroscopy and transmission electron microscopy. α-FeOOH precipitated as a single phase from room temperature to 160 °C in a broad aging time interval. The ratio of the length to the width of α-FeOOH particles depended on the temperature and concentration of the starting FeCl3 solution. Multidomainic character of α-FeOOH particles gradually decreased with an increase in the temperature and time of aging.
Izvorni jezik
Engleski
Znanstvena područja
Fizika, Kemija
POVEZANOST RADA
Ustanove:
Institut "Ruđer Bošković", Zagreb,
Prirodoslovno-matematički fakultet, Zagreb
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus