Pregled bibliografske jedinice broj: 719998
The formation and microstructural properties of uniform α-GaOOH particles and their calcination products
The formation and microstructural properties of uniform α-GaOOH particles and their calcination products // Journal of alloys and compounds, 620 (2015), 217-227 doi:10.1016/j.jallcom.2014.09.134 (međunarodna recenzija, članak, znanstveni)
CROSBI ID: 719998 Za ispravke kontaktirajte CROSBI podršku putem web obrasca
Naslov
The formation and microstructural properties of uniform α-GaOOH particles and their calcination products
Autori
Krehula, Stjepko ; Ristić, Mira ; Kubuki, Shiro ; Iida, Yusuke ; Fabián, Martin ; Musić, Svetozar
Izvornik
Journal of alloys and compounds (0925-8388) 620
(2015);
217-227
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
α-GaOOH; α-Ga2O3; β-Ga2O3; FT-IR; FE-SEM; PL
Sažetak
Uniform α-GaOOH submicron particles of different shapes (spindles, rhombic rods, rhombic prisms, hierarchical particles) were synthesized by simple low-temperature (at 60 °C) or hydrothermal (at 160 °C) precipitation from the mixture of aqueous solutions of gallium(III) chloride and organic alkali tetramethylammonium hydroxide (TMAH) at various pH values (5, 7 or 9). The growth mechanism of these particles was discussed. Crystallographic directions and crystal planes in α-GaOOH particles were identified. Differences in crystallite size, thermal and infrared properties of α-GaOOH particles were observed and discussed. Uniform α-Ga2O3 and β-Ga2O3 particles of the same or similar shapes, containing holes due to dehydroxylation, were obtained by calcination of the corresponding α-GaOOH particles at 500 or 900 °C, respectively. Differences in crystallite size and infrared properties of obtained gallium oxide samples, as well as differences in photoluminescence properties of β-Ga2O3 samples were observed and discussed.
Izvorni jezik
Engleski
Znanstvena područja
Kemija
POVEZANOST RADA
Projekti:
098-0982904-2952 - Sinteza i mikrostruktura metalnih oksida i oksidnih stakala (Ristić, Mira, MZOS ) ( CroRIS)
Ustanove:
Institut "Ruđer Bošković", Zagreb
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus