Pregled bibliografske jedinice broj: 712077
Preparation and characterization of biodegradable polycaprolactone/ titanate nanotubes composites
Preparation and characterization of biodegradable polycaprolactone/ titanate nanotubes composites // 2nd International Conference on Bio-Based Polymers and Composites (BiPoCo 2014) : proceedings / Pukanszky, Bela (ur.).
Budimpešta: Budapest University of Technology and Economics, 2014. str. 1-2 (poster, međunarodna recenzija, cjeloviti rad (in extenso), znanstveni)
CROSBI ID: 712077 Za ispravke kontaktirajte CROSBI podršku putem web obrasca
Naslov
Preparation and characterization of biodegradable polycaprolactone/ titanate nanotubes composites
Autori
Govorčin Bajsić, Emi ; Ocelić Bulatović, Vesna ; Slouf, Miroslav ; Šitum, Ana
Vrsta, podvrsta i kategorija rada
Radovi u zbornicima skupova, cjeloviti rad (in extenso), znanstveni
Izvornik
2nd International Conference on Bio-Based Polymers and Composites (BiPoCo 2014) : proceedings
/ Pukanszky, Bela - Budimpešta : Budapest University of Technology and Economics, 2014, 1-2
Skup
2nd International Conference on Bio-Based Polymers and Composites (2 ; 2014)
Mjesto i datum
Visegrád, Mađarska, 24.08.2014. - 28.08.2014
Vrsta sudjelovanja
Poster
Vrsta recenzije
Međunarodna recenzija
Ključne riječi
Polikaprolakton ; TiO2 ; Ti nanocijevi ; Kompoziti ; Toplinska svojstva
(Polycaprolactone ; TiO2 ; Ti nanotubes ; Composite ; Thermal properties)
Sažetak
The objective of this study was modification of biodegradable polycaprolactone with TiO2 nanotubes as filler in the purpose to improve processing and /or other desired properties. Composites of biodegradable PCL with 0.5, 1.0 and 2.0 wt. % titanate nanotubes were prepared by melt mixing using a laboratory Brabender mixer. Final specimens for all investigations (size 40 mm x 12mm x 1.5 mm) were obtained by compression molding the materials in a hot-plate of a laboratory hydraulic press Dake Model 44-226 at 140°C. TiNT was prepared by hydrothermal synthesis from nano TiO2 particles and dried TiNT nanopowder was employed in preparation of PCL/TiNT composites. The effects of TiNT on the thermal properties (DSC), viscoelastic properties (DMA) and morphology (SEM, LM) were studied. From DSC results, Tm slightly increased, Tc increased while crystallinity (c) decreased with TiNT content in compare with neat PCL. DMA measurements show that the Tg and storage modulus increased in PCL/TiNT composites. SEM and LM results showed that the aggregates were formed.
Izvorni jezik
Engleski
Znanstvena područja
Kemijsko inženjerstvo, Interdisciplinarne tehničke znanosti
POVEZANOST RADA
Projekti:
125-1252971-2578 - Modifikacija i stabilnost višefaznih polimernih sustava (Govorčin-Bajsić, Emi, MZOS ) ( CroRIS)
Ustanove:
Fakultet kemijskog inženjerstva i tehnologije, Zagreb