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Pregled bibliografske jedinice broj: 629202

Pholcodine monohydrate : Crystal structure and polymorphism

Petruševski, Gjorgji; Zbačnik, Marija; Kajdžanoska, Marina; Ugarković, Sonja; Trimčeski, Vase; Kaitner, Branko; Jovanovski, Gligor; Makreski, Petre
Pholcodine monohydrate : Crystal structure and polymorphism // Journal of crystal growth, 375 (2013), 119-124 doi:10.1016/j.jcrysgro.2013.04.031 (međunarodna recenzija, članak, znanstveni)

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Naslov
Pholcodine monohydrate : Crystal structure and polymorphism

Autori
Petruševski, Gjorgji ; Zbačnik, Marija ; Kajdžanoska, Marina ; Ugarković, Sonja ; Trimčeski, Vase ; Kaitner, Branko ; Jovanovski, Gligor ; Makreski, Petre

Izvornik
Journal of crystal growth (0022-0248) 375 (2013); 119-124

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
crystal structure; polymorphism; recrystallization; X-ray diffraction; pharmaceuticals

Sažetak
The first crystal structure elucidation of pholcodine monohydrate, an important antitussive active pharmaceutical ingredient is reported herein.The studied compound crystallizes in the orthorhombic system in the space group P212121. Each H2O molecule is shared by two pholcodine molecules via three strong hydrogen bonds. The detailed crystallization screening from several different organic solvents afforded single crystals with various quality, all exhibiting prism-to-needlelike micromorphology. The investigation of the obtained single crystals by means of several physico-chemical, solid-state instrumental techniques (FT-IR, DSC, TG/DTG and XRPD) proved that pholcodine monohydrate exists in a single crystalline modification, identical to the commercial form of the compound.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
119-1193079-3069 - Novi organski i koordinacijski spojevi - sinteza i suodnos struktura-svojstvo (Kaitner, Branko, MZOS ) ( CroRIS)

Ustanove:
Prirodoslovno-matematički fakultet, Zagreb

Profili:

Avatar Url Marija Zbačnik (autor)

Avatar Url Branko Kaitner (autor)

Poveznice na cjeloviti tekst rada:

Pristup cjelovitom tekstu rada doi www.sciencedirect.com dx.doi.org

Citiraj ovu publikaciju:

Petruševski, Gjorgji; Zbačnik, Marija; Kajdžanoska, Marina; Ugarković, Sonja; Trimčeski, Vase; Kaitner, Branko; Jovanovski, Gligor; Makreski, Petre
Pholcodine monohydrate : Crystal structure and polymorphism // Journal of crystal growth, 375 (2013), 119-124 doi:10.1016/j.jcrysgro.2013.04.031 (međunarodna recenzija, članak, znanstveni)
Petruševski, G., Zbačnik, M., Kajdžanoska, M., Ugarković, S., Trimčeski, V., Kaitner, B., Jovanovski, G. & Makreski, P. (2013) Pholcodine monohydrate : Crystal structure and polymorphism. Journal of crystal growth, 375, 119-124 doi:10.1016/j.jcrysgro.2013.04.031.
@article{article, author = {Petru\v{s}evski, Gjorgji and Zba\v{c}nik, Marija and Kajd\v{z}anoska, Marina and Ugarkovi\'{c}, Sonja and Trim\v{c}eski, Vase and Kaitner, Branko and Jovanovski, Gligor and Makreski, Petre}, year = {2013}, pages = {119-124}, DOI = {10.1016/j.jcrysgro.2013.04.031}, keywords = {crystal structure, polymorphism, recrystallization, X-ray diffraction, pharmaceuticals}, journal = {Journal of crystal growth}, doi = {10.1016/j.jcrysgro.2013.04.031}, volume = {375}, issn = {0022-0248}, title = {Pholcodine monohydrate : Crystal structure and polymorphism}, keyword = {crystal structure, polymorphism, recrystallization, X-ray diffraction, pharmaceuticals} }
@article{article, author = {Petru\v{s}evski, Gjorgji and Zba\v{c}nik, Marija and Kajd\v{z}anoska, Marina and Ugarkovi\'{c}, Sonja and Trim\v{c}eski, Vase and Kaitner, Branko and Jovanovski, Gligor and Makreski, Petre}, year = {2013}, pages = {119-124}, DOI = {10.1016/j.jcrysgro.2013.04.031}, keywords = {crystal structure, polymorphism, recrystallization, X-ray diffraction, pharmaceuticals}, journal = {Journal of crystal growth}, doi = {10.1016/j.jcrysgro.2013.04.031}, volume = {375}, issn = {0022-0248}, title = {Pholcodine monohydrate : Crystal structure and polymorphism}, keyword = {crystal structure, polymorphism, recrystallization, X-ray diffraction, pharmaceuticals} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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