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Pregled bibliografske jedinice broj: 521666

Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe

Gerboles, M.; Buzica, D.; Brown, R.J.C.; Yardley, R.E.; Hanus-Illnar, A.; Salfinger, M.; Vallant, B.; Adriaenssens, E.; Claeys, N.; Roekens, E. et al.
Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe // Atmospheric environment (1994), 45 (2011), 20; 3488-3499 doi:10.1016/j.atmosenv.2010.12.020 (međunarodna recenzija, članak, znanstveni)

CROSBI ID: 521666 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe

Autori
Gerboles, M. ; Buzica, D. ; Brown, R.J.C. ; Yardley, R.E. ; Hanus-Illnar, A. ; Salfinger, M. ; Vallant, B. ; Adriaenssens, E. ; Claeys, N. ; Roekens, E. ; Šega, Krešimir ; Jurasović, Jasna ; Rychlik, S. ; Rabinak, E. ; Tanet, G. ; Passarella, R. ; Pedroni, V. ; Karlsson, V. ; Alleman, L. ; Pfeffer, U. ; Gladtke, D. ; Olschewski, A. ; O’Leary, B. ; O’Dwyer, M. ; Pockeviciute, D. ; Biel-Cwikowska, J. ; Turšič, J.

Izvornik
Atmospheric environment (1994) (1352-2310) 45 (2011), 20; 3488-3499

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
heavy metals; PM10; particulate matter speciation; air quality legislation; uncertainty of measurement

Sažetak
This paper presents the results of an intercomparison exercise for the determination of arsenic (As), cadmium (Cd), nickel (Ni) and lead (Pb) in PM10, which are regulated by the European Directives for ambient air quality. Thirteen laboratories participated, generally using the European reference methods of measurement which consist of a microwave digestion followed by analysis with either ICP-MS or GFAAS. Each participant was asked to analyse five test samples: a liquid Certified Reference Material (CRM), two sub-samples of a NIST dust CRM (one already-digested and one to be digested by the participants) and two loaded filters (one already- digested and one to be digested by the participants). Participants were able to meet the Data Quality Objectives (DQOs) of the European Directives (expanded uncertainties of 25% for Pb and 40% for As, Cd and Ni) for 93% of all test samples, except for the loaded filter that were digested by the participants. In fact, only 76% of DQOs were met for this test sample, the closest to a routine sample analysis in the laboratory. The difficulties in analysing this test sample came mainly from digestion and contamination processes. Satisfactory results were also obtained using other digestion techniques (Soxhlet extraction and high pressure methods) and analytical methods (ICP-OES for Cd, Ni and Pb, EDXRF for Pb and Ni and Voltammetry for As, Ni, and Pb). Participants claimed uncertainties of about 10% for Pb and between 15 and 20% for As, Cd and Ni. These uncertainties were confirmed for 77% of results. The reproducibility of the methods of measurement was between 41 and 54% while repeatability remained between 5 and 12% except for the analysis of As on filters which was up to 20%. The majority of participant results showed higher between-day variability (14 ± 11%) than within-day variability (6.0 ± 5.3%).

Izvorni jezik
Engleski

Znanstvena područja
Javno zdravstvo i zdravstvena zaštita



POVEZANOST RADA

Projekti:
022-0222148-2135 - Izloženost metalima i njihovi učinci u graviditetu i postnatalnom razdoblju (Piasek, Martina, MZOS ) ( CroRIS)
022-0222882-2271 - Vremensko-prostorna razdioba i porijeklo lebdećih čestica u urbanim sredinama (Šega, Krešimir, MZOS ) ( CroRIS)

Ustanove:
Institut za medicinska istraživanja i medicinu rada, Zagreb

Profili:

Avatar Url Jasna Jurasović (autor)

Avatar Url Krešimir Šega (autor)

Poveznice na cjeloviti tekst rada:

Pristup cjelovitom tekstu rada doi www.sciencedirect.com dx.doi.org dx.doi.org

Citiraj ovu publikaciju:

Gerboles, M.; Buzica, D.; Brown, R.J.C.; Yardley, R.E.; Hanus-Illnar, A.; Salfinger, M.; Vallant, B.; Adriaenssens, E.; Claeys, N.; Roekens, E. et al.
Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe // Atmospheric environment (1994), 45 (2011), 20; 3488-3499 doi:10.1016/j.atmosenv.2010.12.020 (međunarodna recenzija, članak, znanstveni)
Gerboles, M., Buzica, D., Brown, R., Yardley, R., Hanus-Illnar, A., Salfinger, M., Vallant, B., Adriaenssens, E., Claeys, N. & Roekens, E. (2011) Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe. Atmospheric environment (1994), 45 (20), 3488-3499 doi:10.1016/j.atmosenv.2010.12.020.
@article{article, author = {Gerboles, M. and Buzica, D. and Brown, R.J.C. and Yardley, R.E. and Hanus-Illnar, A. and Salfinger, M. and Vallant, B. and Adriaenssens, E. and Claeys, N. and Roekens, E. and \v{S}ega, Kre\v{s}imir and Jurasovi\'{c}, Jasna and Rychlik, S. and Rabinak, E. and Tanet, G. and Passarella, R. and Pedroni, V. and Karlsson, V. and Alleman, L. and Pfeffer, U. and Gladtke, D. and Olschewski, A. and O’Leary, B. and O’Dwyer, M. and Pockeviciute, D. and Biel-Cwikowska, J. and Tur\v{s}i\v{c}, J.}, year = {2011}, pages = {3488-3499}, DOI = {10.1016/j.atmosenv.2010.12.020}, keywords = {heavy metals, PM10, particulate matter speciation, air quality legislation, uncertainty of measurement}, journal = {Atmospheric environment (1994)}, doi = {10.1016/j.atmosenv.2010.12.020}, volume = {45}, number = {20}, issn = {1352-2310}, title = {Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe}, keyword = {heavy metals, PM10, particulate matter speciation, air quality legislation, uncertainty of measurement} }
@article{article, author = {Gerboles, M. and Buzica, D. and Brown, R.J.C. and Yardley, R.E. and Hanus-Illnar, A. and Salfinger, M. and Vallant, B. and Adriaenssens, E. and Claeys, N. and Roekens, E. and \v{S}ega, Kre\v{s}imir and Jurasovi\'{c}, Jasna and Rychlik, S. and Rabinak, E. and Tanet, G. and Passarella, R. and Pedroni, V. and Karlsson, V. and Alleman, L. and Pfeffer, U. and Gladtke, D. and Olschewski, A. and O’Leary, B. and O’Dwyer, M. and Pockeviciute, D. and Biel-Cwikowska, J. and Tur\v{s}i\v{c}, J.}, year = {2011}, pages = {3488-3499}, DOI = {10.1016/j.atmosenv.2010.12.020}, keywords = {heavy metals, PM10, particulate matter speciation, air quality legislation, uncertainty of measurement}, journal = {Atmospheric environment (1994)}, doi = {10.1016/j.atmosenv.2010.12.020}, volume = {45}, number = {20}, issn = {1352-2310}, title = {Interlaboratory comparison exercise for the determination of As, Cd, Ni and Pb in PM10 in Europe}, keyword = {heavy metals, PM10, particulate matter speciation, air quality legislation, uncertainty of measurement} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

Uključenost u ostale bibliografske baze podataka::


  • Analytical Abstracts
  • BIOSIS Previews (Biological Abstracts)
  • CA Search (Chemical Abstracts)
  • EMBASE (Excerpta Medica)
  • Geobase
  • INSPEC
  • Meteorological and Geoastrophysical Abstracts
  • Acid Precipitation Digest
  • Air Pollution Titles
  • Cambridge Scientific Abstracts
  • BIOBASE
  • Pascal/CNRS
  • SCISEARCH

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