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Pregled bibliografske jedinice broj: 458413

Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection

Čukelj, Nikolina; Jakaša, Ivone; Sarajlija, Hrvoje; Novotni, Dubravka; Ćurić, Duška
Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection // Talanta, 84 (2011), 127-132 doi:10.1016/j.talanta.2010.12.025 (međunarodna recenzija, članak, znanstveni)

CROSBI ID: 458413 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection

Autori
Čukelj, Nikolina ; Jakaša, Ivone ; Sarajlija, Hrvoje ; Novotni, Dubravka ; Ćurić, Duška

Izvornik
Talanta (0039-9140) 84 (2011); 127-132

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
lignans ; wheat bran ; derivatization ; GC-ECD ; internal standard ; validation

Sažetak
Whole grain cereals are an important source of bioavailable lignans, the group of compounds with potential anti-cancerogenic, antioxidant, anti-proliferative, pro-apoptotic, and antiangiogenic properties. The aim of this work was to develop a sensitive method for determination of wheat bran lignans. The analysis of lignans secoisolariciresinol, hydroxymatairesinol, lariciresinol, matairesinol, pinoresinol, syringaresinol is based on derivatization with pentafluoropropionic anhydride (PFPA) and gas chromatography-electron capture detection (GC-ECD), using styrene glycol as internal standard. To our knowledge, this is the first time that EC detection has been used for lignan analysis. The results show that the technique is reproducible and sensitive enough for detecting lignans in wheat at parts-per-billion(ppb) levels, except for hydroxymatairesinol. The method developed showed good recovery (85–105%) and precision (4–20%) for five types of lignans and thus represents a simpler and more affordable alternative to state-of-the-art wheat lignan liquid chromatography tandem mass spectrometry (LC–MS/MS) analysis.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Prehrambena tehnologija



POVEZANOST RADA

Projekti:
058-0580696-0702 - Lignani u žitaricama, uljaricama, soji i integralnim pekarskim proizvodima (Ćurić, Duška, MZOS ) ( CroRIS)

Ustanove:
Prehrambeno-biotehnološki fakultet, Zagreb

Profili:

Avatar Url Duška Ćurić (autor)

Avatar Url Dubravka Novotni (autor)

Avatar Url Ivone Jakasa (autor)

Avatar Url Hrvoje Sarajlija (autor)

Avatar Url Nikolina Čukelj Mustač (autor)

Poveznice na cjeloviti tekst rada:

doi www.sciencedirect.com www.sciencedirect.com www.sciencedirect.com

Citiraj ovu publikaciju:

Čukelj, Nikolina; Jakaša, Ivone; Sarajlija, Hrvoje; Novotni, Dubravka; Ćurić, Duška
Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection // Talanta, 84 (2011), 127-132 doi:10.1016/j.talanta.2010.12.025 (međunarodna recenzija, članak, znanstveni)
Čukelj, N., Jakaša, I., Sarajlija, H., Novotni, D. & Ćurić, D. (2011) Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection. Talanta, 84, 127-132 doi:10.1016/j.talanta.2010.12.025.
@article{article, author = {\v{C}ukelj, Nikolina and Jaka\v{s}a, Ivone and Sarajlija, Hrvoje and Novotni, Dubravka and \'{C}uri\'{c}, Du\v{s}ka}, year = {2011}, pages = {127-132}, DOI = {10.1016/j.talanta.2010.12.025}, keywords = {lignans, wheat bran, derivatization, GC-ECD, internal standard, validation}, journal = {Talanta}, doi = {10.1016/j.talanta.2010.12.025}, volume = {84}, issn = {0039-9140}, title = {Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection}, keyword = {lignans, wheat bran, derivatization, GC-ECD, internal standard, validation} }
@article{article, author = {\v{C}ukelj, Nikolina and Jaka\v{s}a, Ivone and Sarajlija, Hrvoje and Novotni, Dubravka and \'{C}uri\'{c}, Du\v{s}ka}, year = {2011}, pages = {127-132}, DOI = {10.1016/j.talanta.2010.12.025}, keywords = {lignans, wheat bran, derivatization, GC-ECD, internal standard, validation}, journal = {Talanta}, doi = {10.1016/j.talanta.2010.12.025}, volume = {84}, issn = {0039-9140}, title = {Identification and quantification of lignans in wheat bran by gas chromatography-electron capture detection}, keyword = {lignans, wheat bran, derivatization, GC-ECD, internal standard, validation} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE

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