Pregled bibliografske jedinice broj: 367048
Numerical Modelling of Sample : Furnace Thermal Lag in Dynamic Mechanical Analyser
Numerical Modelling of Sample : Furnace Thermal Lag in Dynamic Mechanical Analyser // Journal of thermal analysis and calorimetry, 100 (2010), 1; 337-345 doi:10.1007/s10973-009-0447-z (međunarodna recenzija, članak, znanstveni)
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Naslov
Numerical Modelling of Sample : Furnace Thermal Lag in Dynamic Mechanical Analyser
Autori
Sućeska, Muhamed ; Zhi-Yue, Liu ; Matečić Mušanić, Sanja ; Fiamengo, Ivona
Izvornik
Journal of thermal analysis and calorimetry (1388-6150) 100
(2010), 1;
337-345
Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni
Ključne riječi
thermal methods; dynamic mechanical analysis; heat conduction equation; thermal lag; thermal gradient; heat transfer coefficient
Sažetak
Due to dynamic nature of processes taking place during the experiment (chemical reaction and physical processes, heat flow, gas flow, etc.) the results obtained by thermal methods may considerably depend on the conditions used during the experiment. Therefore, whenever the results of thermal analysis are reported, the experimental conditions used should be stated. In this paper we have studied the heat transfer from the furnace to the sample and through the sample during dynamic mechanical analysis (DMA) measurements. Numerical modelling of the heat transfer was done using an own computer program based on the heat conduction equation, solved numerically applying the finite difference methods. The calculated values of the thermal lag between the furnace and the sample were compared with the values experimentally determined on samples of a composite polymeric energetic material (double-base rocket propellant). Also, the temperature distribution within the sample as a function of the heating rate was analysed using the same numerical model. It was found out that using this model and temperature dependent heat transfer coefficient, experimentally obtained values of the thermal lag between the furnace and the sample can be satisfactory described. It was also shown that even at slow heating rates, such is e.g. 2 oC min-1, the thermal lag between the furnace and the sample can reach several degrees, while the thermal gradient within 3 mm thick rectangular sample can reach 0.4 oC
Izvorni jezik
Engleski
Znanstvena područja
Kemija, Kemijsko inženjerstvo
POVEZANOST RADA
Projekti:
192-1252971-1982 - Istraživanje procesa starenja i predikcija životnog vijeka materijala (Sućeska, Muhamed, MZOS ) ( CroRIS)
Ustanove:
Brodarski institut d.o.o.
Citiraj ovu publikaciju:
Časopis indeksira:
- Current Contents Connect (CCC)
- Web of Science Core Collection (WoSCC)
- Science Citation Index Expanded (SCI-EXP)
- SCI-EXP, SSCI i/ili A&HCI
- Scopus