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Pregled bibliografske jedinice broj: 344159

Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives

Krištafor, Svjetlana; Gazivoda, Tatjana; Cetina, Mario; Makuc, Damjan; Plavec, Janez; Raić-Malić, Silvana
Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives // Journal of molecular structure, 923 (2009), 1-3; 19-23 doi:10.1016/j.molstruc.2008.12.037 (međunarodna recenzija, članak, znanstveni)

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Naslov
Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives

Autori
Krištafor, Svjetlana ; Gazivoda, Tatjana ; Cetina, Mario ; Makuc, Damjan ; Plavec, Janez ; Raić-Malić, Silvana

Izvornik
Journal of molecular structure (0022-2860) 923 (2009), 1-3; 19-23

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
C-6 fluoroalkylated pyrimidines ; X-ray crystal structure analysis ; pi• • • pi interactions

Sažetak
C-6 substituted fluoroalkenyl 2, 4-dimethoxypyrimidine derivative (4) was synthesized by lithiation of 2, 4-dimethoxy-6-methylpyrimidine (3) and subsequent reaction of thus obtained organolithium intermediate with ethyl pentafluoropropionate. The novel 2, 4-pyrimidinedione containing 3, 3, 4, 4, 4-pentafluoro-1-butenyl side chain (5) was prepared by demethoxylation of 4 using sodium iodide and chlorotrimethylsilane. The structures of 4 and 5 were confirmed by 1H, 13C and 19F NMR spectra, as well as IR spectra. The structure of 4 was also unambiguously confirmed by X-ray crystal structure analysis. The molecules of 4 are weakly linked by aromatic pi• • • pi stacking interactions into infinite chains parallel to the a axis.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
MZOS-119-1193079-3069 - Novi organski i koordinacijski spojevi - sinteza i suodnos struktura-svojstvo (Kaitner, Branko, MZOS ) ( CroRIS)
MZOS-125-0982464-2925 - Razvoj i primjena novih molekula u pozitron-emisijskoj tomografiji (PET) (Raić-Malić, Silvana, MZOS ) ( CroRIS)

Ustanove:
Tekstilno-tehnološki fakultet, Zagreb,
Prirodoslovno-matematički fakultet, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb

Profili:

Avatar Url Svjetlana Krištafor (autor)

Avatar Url Silvana Raić-Malić (autor)

Avatar Url Mario Cetina (autor)

Avatar Url Tatjana Gazivoda Kraljević (autor)

Poveznice na cjeloviti tekst rada:

doi doi.org www.sciencedirect.com

Citiraj ovu publikaciju:

Krištafor, Svjetlana; Gazivoda, Tatjana; Cetina, Mario; Makuc, Damjan; Plavec, Janez; Raić-Malić, Silvana
Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives // Journal of molecular structure, 923 (2009), 1-3; 19-23 doi:10.1016/j.molstruc.2008.12.037 (međunarodna recenzija, članak, znanstveni)
Krištafor, S., Gazivoda, T., Cetina, M., Makuc, D., Plavec, J. & Raić-Malić, S. (2009) Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives. Journal of molecular structure, 923 (1-3), 19-23 doi:10.1016/j.molstruc.2008.12.037.
@article{article, author = {Kri\v{s}tafor, Svjetlana and Gazivoda, Tatjana and Cetina, Mario and Makuc, Damjan and Plavec, Janez and Rai\'{c}-Mali\'{c}, Silvana}, year = {2009}, pages = {19-23}, DOI = {10.1016/j.molstruc.2008.12.037}, keywords = {C-6 fluoroalkylated pyrimidines, X-ray crystal structure analysis, pi• • • pi interactions}, journal = {Journal of molecular structure}, doi = {10.1016/j.molstruc.2008.12.037}, volume = {923}, number = {1-3}, issn = {0022-2860}, title = {Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives}, keyword = {C-6 fluoroalkylated pyrimidines, X-ray crystal structure analysis, pi• • • pi interactions} }
@article{article, author = {Kri\v{s}tafor, Svjetlana and Gazivoda, Tatjana and Cetina, Mario and Makuc, Damjan and Plavec, Janez and Rai\'{c}-Mali\'{c}, Silvana}, year = {2009}, pages = {19-23}, DOI = {10.1016/j.molstruc.2008.12.037}, keywords = {C-6 fluoroalkylated pyrimidines, X-ray crystal structure analysis, pi• • • pi interactions}, journal = {Journal of molecular structure}, doi = {10.1016/j.molstruc.2008.12.037}, volume = {923}, number = {1-3}, issn = {0022-2860}, title = {Synthesis and structural characterization of the C-6 fluoroalkylated pyrimidine derivatives}, keyword = {C-6 fluoroalkylated pyrimidines, X-ray crystal structure analysis, pi• • • pi interactions} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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