Naslov
Optimization of Sintering Process of Alumina Ceramics Using Response Surface Methodology

Autori
Darko, Landek ; Ćurković, Lidija ; Gabelica, Ivana ; Kerolli Mustafa, Mihone ; Žmak, Irena

Izvornik
Sustainability (2071-1050) 13 (2021), 12; 1-14

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, ostalo

Ključne riječi
alumina ; slip casting ; sintering ; Box–Behnken design ; response surface method

Sažetak
In this work, alumina (Al2O3) ceramics were prepared using an environmentally friendly slip casting method. To this end, highly concentrated (70 wt.%) aqueous suspensions of alumina (Al2O3) were prepared with different amounts of the ammonium salt of a polycarboxylic acid, Dolapix CE 64, as an electrosteric dispersant. The stability of highly concentrated Al2O3 aqueous suspensions was monitored by viscosity measurements. Green bodies (ceramics before sintering) were obtained by pouring the stable Al2O3 aqueous suspensions into dry porous plaster molds. The obtained Al2O3 ceramic green bodies were sintered in the electric furnace. Analysis of the effect of three sintering parameters (sintering temperature, heating rate and holding time) on the density of alumina ceramics was performed using the response surface methodology (RSM), based on experimental data obtained according to Box–Behnken experimental design, using the software Design-Expert. From the statistical analysis, linear and nonlinear models with added first-order interaction were developed for prediction and optimization of density- dependent variables: sintering temperature, heating rate and holding time.

Izvorni jezik
Engleski

Znanstvena područja
Kemijsko inženjerstvo, Strojarstvo, Temeljne tehničke znanosti

POVEZANOST RADA