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Pregled bibliografske jedinice broj: 1030410

Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes

Bjelopetrović, Alen; Robić, Marko; Halasz, Ivan; Babić, Darko; Juribašić Kulcsar, Marina; Ćurić, Manda
Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes // Organometallics, 38 (2019), 22; 4479-4484 doi:10.1021/acs.organomet.9b00626 (međunarodna recenzija, članak, znanstveni)

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Naslov
Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes

Autori
Bjelopetrović, Alen ; Robić, Marko ; Halasz, Ivan ; Babić, Darko ; Juribašić Kulcsar, Marina ; Ćurić, Manda

Izvornik
Organometallics (0276-7333) 38 (2019), 22; 4479-4484

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
solvent-free ; anion substitution ; organopalladium compounds ; cyclopaladates ; azobenzenes ; mechanochemistry

Sažetak
Solvent-free ball-milling method for substitution of anionic ligands in organopalladium compounds was developed. Reactions of acetate, acetylacetonate, chloride or tetrafluoroborate of mono- or dicyclopalladated azobenzenes with alkali salts of chloride acetate and acetylacetonate yielded target products, some of which could not be obtained via direct C–H bond activation by Pd(II) precursors. The formation of products was monitored in situ by Raman spectroscopy and ex situ by NMR and IR spectroscopies and PXRD. The reported solid-state pathway provides an easy access to organopalladium derivatives in high yields and in shorter reaction times than solvent-based protocols.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
IP-2014-09-7984 - Zelena sinteza organopaladijevih foto-osjetljivih spojeva (GREENSENS) (Ćurić, Manda, HRZZ - 2014-09) ( CroRIS)

Ustanove:
Institut "Ruđer Bošković", Zagreb

Profili:

Avatar Url Ivan Halasz (autor)

Avatar Url Alen Bjelopetrović (autor)

Avatar Url Marina Juribašić Kulcsar (autor)

Avatar Url Marko Robić (autor)

Avatar Url Manda Ćurić (autor)

Avatar Url Darko Babić (autor)

Poveznice na cjeloviti tekst rada:

doi doi.org pubs.acs.org

Citiraj ovu publikaciju:

Bjelopetrović, Alen; Robić, Marko; Halasz, Ivan; Babić, Darko; Juribašić Kulcsar, Marina; Ćurić, Manda
Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes // Organometallics, 38 (2019), 22; 4479-4484 doi:10.1021/acs.organomet.9b00626 (međunarodna recenzija, članak, znanstveni)
Bjelopetrović, A., Robić, M., Halasz, I., Babić, D., Juribašić Kulcsar, M. & Ćurić, M. (2019) Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes. Organometallics, 38 (22), 4479-4484 doi:10.1021/acs.organomet.9b00626.
@article{article, author = {Bjelopetrovi\'{c}, Alen and Robi\'{c}, Marko and Halasz, Ivan and Babi\'{c}, Darko and Juriba\v{s}i\'{c} Kulcsar, Marina and \'{C}uri\'{c}, Manda}, year = {2019}, pages = {4479-4484}, DOI = {10.1021/acs.organomet.9b00626}, keywords = {solvent-free, anion substitution, organopalladium compounds, cyclopaladates, azobenzenes, mechanochemistry}, journal = {Organometallics}, doi = {10.1021/acs.organomet.9b00626}, volume = {38}, number = {22}, issn = {0276-7333}, title = {Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes}, keyword = {solvent-free, anion substitution, organopalladium compounds, cyclopaladates, azobenzenes, mechanochemistry} }
@article{article, author = {Bjelopetrovi\'{c}, Alen and Robi\'{c}, Marko and Halasz, Ivan and Babi\'{c}, Darko and Juriba\v{s}i\'{c} Kulcsar, Marina and \'{C}uri\'{c}, Manda}, year = {2019}, pages = {4479-4484}, DOI = {10.1021/acs.organomet.9b00626}, keywords = {solvent-free, anion substitution, organopalladium compounds, cyclopaladates, azobenzenes, mechanochemistry}, journal = {Organometallics}, doi = {10.1021/acs.organomet.9b00626}, volume = {38}, number = {22}, issn = {0276-7333}, title = {Facile Mechanochemical Anion Substitution in Cyclopalladated Azo-benzenes}, keyword = {solvent-free, anion substitution, organopalladium compounds, cyclopaladates, azobenzenes, mechanochemistry} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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