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Pregled bibliografske jedinice broj: 989107

The utilization of ball milling in synthesis of aryl guanidines through guanidinylation and N- Boc-deprotection sequence


Đud, Mateja; Glasovac, Zoran; Margetić, Davor
The utilization of ball milling in synthesis of aryl guanidines through guanidinylation and N- Boc-deprotection sequence // Tetrahedron, 75 (2019), 1; 109-115 (međunarodna recenzija, članak, znanstveni)


Naslov
The utilization of ball milling in synthesis of aryl guanidines through guanidinylation and N- Boc-deprotection sequence

Autori
Đud, Mateja ; Glasovac, Zoran ; Margetić, Davor

Izvornik
Tetrahedron (0040-4020) 75 (2019), 1; 109-115

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Guanidines ; Amines ; Guanidinylation ; Mechanochemistry ; N-Boc deprotection

Sažetak
Solid state ball milling was used in guanidinylation reactions of aromatic amines with N, N′-Di-Boc-1H-pyrazole-1-carboxamidine reagent. Reaction conditions are advantageous, and in general reactions proceed in significantly shorter reaction times and in higher yields than under the conventional solution conditions. Mechanochemical conditions were also successfully applied to the cleavage of N-Boc protecting group.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekt / tema
HRZZ-IP-2013-11-9310 - Nekovalentne interakcije u dizajnu novih fotoosjetljivih molekula (Davor Margetić, )

Ustanove
Institut "Ruđer Bošković", Zagreb

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus