Simple and Efficient Large-scale Metal-free Synthesis of o-(5-Formyl-2-thienyl)benzonitrile and o-(5-Formyl-2-furyl)benzonitrile (CROSBI ID 248724)
Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija
Podaci o odgovornosti
Lovrić, Marija ; Majed Tibi, Mohamed ; Filipan, Mirela ; Cepanec, Ivica ; Litvić, Mladen
engleski
Simple and Efficient Large-scale Metal-free Synthesis of o-(5-Formyl-2-thienyl)benzonitrile and o-(5-Formyl-2-furyl)benzonitrile
Modification of the Gomberg-Bachmann-Hey reaction was shown to be the best way for simple and efficient large-scale metal-free synthesis of o-(5-Formyl-2-thienyl)benzonitrile and o-(5-formyl-2-furyl)benzonitrile starting from the respective diazonium salts 2- (methoxycarbonyl)benzenediazonium tetrafluoroborate in thiophene or furan as solvent and reagents. The transformation of the resulting intermediates to the target aldehydes was easily performed by using suitable reagents and reaction conditions.
Gomberg-Bachmann-Hey reaction, o-(5-formyl-2-thienyl)benzonitrile, o-(5-formyl-2-furyl)benzonitrile
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Podaci o izdanju
50 (1)
2018.
81-90
objavljeno
0030-4948
1945-5453
10.1080/00304948.2018.1405334