2,3-Dimethylbenzoxazolium Methosulfate (CROSBI ID 247083)
Prilog u časopisu | kratko priopćenje | međunarodna recenzija
Podaci o odgovornosti
Kurutos, Atanas ; Gadjev, Nikolai ; Šmidlehner, Tamara ; Minkovska, Stela ; Piantanida, Ivo ; Deligeorgiev, Todor
engleski
2,3-Dimethylbenzoxazolium Methosulfate
An economically benign solvent-free approach to synthesise 2, 3-dimethylbenzoxazolium methosulfate is reported in the present work. The title compound is derived from 2- methylbenzoxazole reacting with a slight excess of dimethylsulfate, at room temperature. The reaction proceeds via an intrinsic exothermic reaction, and the benzoxazolium salt crystallized after a short time into a white crystalline form. The product was filtered off and washed with acetone and diethyl ether to provide the desired product in 89% yield. The target compound was evaluated by ESI/MS analysis.
2-methylbenzoxazole ; dimethylsulfate ; 2, 3-dimethylbenzoxazolium methosulfate
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