Napredna pretraga

Pregled bibliografske jedinice broj: 919845

2, 3-Dimethylbenzoxazolium Methosulfate


Kurutos, Atanas; Gadjev, Nikolai; Šmidlehner, Tamara; Minkovska, Stela; Piantanida, Ivo; Deligeorgiev, Todor
2, 3-Dimethylbenzoxazolium Methosulfate // Molbank, 2016 (2016), 1; M889, 3 doi:10.3390/M889 (međunarodna recenzija, članak, znanstveni)


Naslov
2, 3-Dimethylbenzoxazolium Methosulfate

Autori
Kurutos, Atanas ; Gadjev, Nikolai ; Šmidlehner, Tamara ; Minkovska, Stela ; Piantanida, Ivo ; Deligeorgiev, Todor

Izvornik
Molbank (1422-8599) 2016 (2016), 1; M889, 3

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
2-methylbenzoxazole ; dimethylsulfate ; 2, 3-dimethylbenzoxazolium methosulfate

Sažetak
An economically benign solvent-free approach to synthesise 2, 3-dimethylbenzoxazolium methosulfate is reported in the present work. The title compound is derived from 2-methylbenzoxazole reacting with a slight excess of dimethylsulfate, at room temperature. The reaction proceeds via an intrinsic exothermic reaction, and the benzoxazolium salt crystallized after a short time into a white crystalline form. The product was filtered off and washed with acetone and diethyl ether to provide the desired product in 89% yield. The target compound was evaluated by ESI/MS analysis.

Izvorni jezik
Engleski



POVEZANOST RADA


Projekt / tema
HRZZ-IP-2013-11-1477 - Višenamjensko očitavanje DNA / RNA sekundarne strukture molekularnim kemijskim senzorima (Ivo Piantanida, )

Ustanove
Institut "Ruđer Bošković", Zagreb

Časopis indeksira:


  • Scopus


Citati