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In situ monitoring as tools to study mechanochemical reactions (CROSBI ID 651860)

Prilog sa skupa u zborniku | sažetak izlaganja sa skupa

Halasz, Ivan ; Užarević, Krunoslav ; Lukin, Stipe ; Friščić, Tomislav In situ monitoring as tools to study mechanochemical reactions // INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying: Program and Abstracts / Šepelák, Vladimír (ur.). Košice, 2017. str. 48-48

Podaci o odgovornosti

Halasz, Ivan ; Užarević, Krunoslav ; Lukin, Stipe ; Friščić, Tomislav

engleski

In situ monitoring as tools to study mechanochemical reactions

We will here describe the development of mechanistic understanding from the first in situ monitoring by synchrotron powder X-ray difraction [1, 2], followed by laboratory Raman in situ monitoring [3, 4] and finally focus on the most recent quantitative evaluation from tandem in situ monitoring combining the two techniques in a high-throughput approach enabling quantitative assessment and kinetic analysis even in systems involving novel and short-lived phases of unknown crystal structures. These recent results provide the necessary infrastructure for a thorough mechanistic description of mechanochemical milling reactions which was thus far hindered mainly by the inability of their quantitative evaluation. We will address also the issue of the temperature of the reaction mixture and its influence of reaction kinetics and mechanisms. Quantitative assessment from tandem in situ monitoring, performed in seconds-time resolution, establishes also Raman monitoring as a quantitative in situ technique that is readily implemented in a conventional laboratory.

mechanochemistry ; in situ monitoring ; Raman spectroscopy ; powder diffraction ; quantitative analysis

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Podaci o prilogu

48-48.

2017.

objavljeno

Podaci o matičnoj publikaciji

INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying: Program and Abstracts

Šepelák, Vladimír

Košice:

Podaci o skupu

INCOME2017, 9th International Conference on Mechanochemistry and Mechanical Alloying

predavanje

03.09.2017-07.09.2017

Košice, Slovačka

Povezanost rada

Kemija