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Pregled bibliografske jedinice broj: 808355

In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer


Huskić, Igor; Christopherson, Jan-Constantin; Užarević, Krunoslav; Friščić, Tomislav
In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer // Chemical communications, 52 (2016), 5120-5123 doi:10.1039/C6CC01583B (međunarodna recenzija, članak, znanstveni)


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Naslov
In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer

Autori
Huskić, Igor ; Christopherson, Jan-Constantin ; Užarević, Krunoslav ; Friščić, Tomislav

Izvornik
Chemical communications (1359-7345) 52 (2016); 5120-5123

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Vapour-induced reactions ; solid-state transformations ; in situ monitoring ; pharmaceutical materials ; polymorphism ; intermediates

Sažetak
We describe a simple setup for in situ continuous monitoring of vapour-induced transformations of organic solids using a benchtop powder X-ray diffractometer. Proof-of- principle application of this setup to model pharmaceutical cocrystals reveals complex reactivity, transformations of reaction intermediates within minutes, and a simple route to the rarely observed monoclinic form of the pharmaceutical cocrystal of carbamazepine and saccharin.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekt / tema
FP7-NEWFELPRO-62

Ustanove
Institut "Ruđer Bošković", Zagreb

Profili:

Avatar Url Krunoslav Užarević (autor)

Citiraj ovu publikaciju

Huskić, Igor; Christopherson, Jan-Constantin; Užarević, Krunoslav; Friščić, Tomislav
In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer // Chemical communications, 52 (2016), 5120-5123 doi:10.1039/C6CC01583B (međunarodna recenzija, članak, znanstveni)
Huskić, I., Christopherson, J., Užarević, K. & Friščić, T. (2016) In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer. Chemical communications, 52, 5120-5123 doi:10.1039/C6CC01583B.
@article{article, year = {2016}, pages = {5120-5123}, DOI = {10.1039/C6CC01583B}, keywords = {Vapour-induced reactions, solid-state transformations, in situ monitoring, pharmaceutical materials, polymorphism, intermediates}, journal = {Chemical communications}, doi = {10.1039/C6CC01583B}, volume = {52}, issn = {1359-7345}, title = {In situ monitoring of vapour-induced assembly of pharmaceutical cocrystals using a benchtop powder X-ray diffractometer}, keyword = {Vapour-induced reactions, solid-state transformations, in situ monitoring, pharmaceutical materials, polymorphism, intermediates} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • Arts & Humanities Citation Index (A&HCI)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE


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