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In situ monitoring and mechanism of the mechanochemical formation of a microporous MOF-74 framework (CROSBI ID 225326)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Julien, Patrick A. ; Užarević, Krunoslav ; Katsenis, Athanassios D. ; Kimber, Simon A.J. ; Wang, Timothy ; Farha, Omar K. ; Zhang, Yuancheng ; Casaban, José ; Germann, Luzia ; Etter, Martin et al. In situ monitoring and mechanism of the mechanochemical formation of a microporous MOF-74 framework // Journal of the American Chemical Society, 138 (2016), 9; 2929-2932. doi: 10.1021/jacs.5b13038

Podaci o odgovornosti

Julien, Patrick A. ; Užarević, Krunoslav ; Katsenis, Athanassios D. ; Kimber, Simon A.J. ; Wang, Timothy ; Farha, Omar K. ; Zhang, Yuancheng ; Casaban, José ; Germann, Luzia ; Etter, Martin ; Dinnebier, Robert E. ; James, Stuart L. ; Halasz, Ivan ; Friščić, Tomislav

engleski

In situ monitoring and mechanism of the mechanochemical formation of a microporous MOF-74 framework

Mechanochemistry provides a rapid, efficient route to metal-organic framework Zn-MOF-74 directly from a metal oxide and without bulk solvent. In situ synchrotron X-ray diffraction monitoring of the reaction course reveals two new phases and an unusual step-wise process in which a close-packed intermediate reacts to form the open framework. The reaction can be performed on a gram scale to yield a highly porous material after activation.

mechanochemistry ; in situ monitoring ; X-ray diffraction ; mechanism ; MOF-74 ; metal-organic framework

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Podaci o izdanju

138 (9)

2016.

2929-2932

objavljeno

0002-7863

10.1021/jacs.5b13038

Povezanost rada

Kemija

Poveznice