Development of C-N coupling using mechanochemistry: catalytic coupling of arylsulfonamides and carbodiimides (CROSBI ID 217398)
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Podaci o odgovornosti
Tan, Davin ; Mottillo, Cristina ; Katsenis, Athanassios D. ; Štrukil, Vjekoslav ; Friščić, Tomislav
engleski
Development of C-N coupling using mechanochemistry: catalytic coupling of arylsulfonamides and carbodiimides
Reported herein is the mechanochemical synthesis of sulfonyl guanidines, a family of molecules which are relevant as pharmaceuticals and herbicides, by direct coupling of sulfonamides and aromatic or aliphatic carbodiimides. Attempts to conduct the coupling in solution have either failed or given very low conversions, thus demonstrating mechanochemistry as the necessary component for the discovery of this synthetic strategy.
C-N coupling; copper; heterogeneous catalysis; mechanosynthesis; synthetic methods
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Podaci o izdanju
53 (35)
2014.
9321-9324
objavljeno
1433-7851
10.1002/anie.201404120