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Benzothiazolyl and Benzimidazolyl Substituted 1-Iminoisoindolines: Synthesis, Mechanistic Studies and Crystal Structure Determination


Sović, Irena; Orehovec, Iva; Stilinović, Vladimir; Basarić, Nikola; Karminski-Zamola, Grace
Benzothiazolyl and Benzimidazolyl Substituted 1-Iminoisoindolines: Synthesis, Mechanistic Studies and Crystal Structure Determination // Monatshefte für Chemie, 147 (2016), 10; 1825-1837 doi:10.1007/s00706-016-1796-5 (međunarodna recenzija, članak, znanstveni)


Naslov
Benzothiazolyl and Benzimidazolyl Substituted 1-Iminoisoindolines: Synthesis, Mechanistic Studies and Crystal Structure Determination

Autori
Sović, Irena ; Orehovec, Iva ; Stilinović, Vladimir ; Basarić, Nikola ; Karminski-Zamola, Grace

Izvornik
Monatshefte für Chemie (0026-9247) 147 (2016), 10; 1825-1837

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Heterocycles ; Reaction mechanisms ; Schiff bases ; X-Ray structure determination

Sažetak
New benzothiazolyl and benzimidazolyl substituted 1-iminoisoidolines are prepared in the reaction of o-phthalaldehyde and substituted 2-aminobenzothiazoles and 2-aminobenzimidazoles. The optimization of these reactions is discussed and the reaction mechanisms are proposed based on the experimental findings. Isoindolines with other heterocyclic substituents are prepared as a confirmation of the proposed mechanisms. Molecular and crystal structures of several prepared compounds are determined by a single crystal X-ray diffraction. These structures are found to be in line with projections based on the chemical and spectroscopic properties, and thus offer an additional confirmation of the proposed reaction mechanisms.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekt / tema
HRZZ-IP-2013-11-5596 - SINTEZA I CITOSTATSKA ISPITIVANJA BIBLIOTEKE NOVIH DUŠIKOVIH HETEROCIKLA (Silvana Raić-Malić, )

Ustanove
Institut "Ruđer Bošković", Zagreb,
Prirodoslovno-matematički fakultet, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • Arts & Humanities Citation Index (A&HCI)
    • SCI-EXP, SSCI i/ili A&HCI


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