Benzothiazolyl and Benzimidazolyl Substituted 1-Iminoisoindolines: Synthesis, Mechanistic Studies and Crystal Structure Determination (CROSBI ID 215943)
Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija
Podaci o odgovornosti
Sović, Irena ; Orehovec, Iva ; Stilinović, Vladimir ; Basarić, Nikola ; Karminski-Zamola, Grace
engleski
Benzothiazolyl and Benzimidazolyl Substituted 1-Iminoisoindolines: Synthesis, Mechanistic Studies and Crystal Structure Determination
New benzothiazolyl and benzimidazolyl substituted 1-iminoisoidolines are prepared in the reaction of o-phthalaldehyde and substituted 2-aminobenzothiazoles and 2-aminobenzimidazoles. The optimization of these reactions is discussed and the reaction mechanisms are proposed based on the experimental findings. Isoindolines with other heterocyclic substituents are prepared as a confirmation of the proposed mechanisms. Molecular and crystal structures of several prepared compounds are determined by a single crystal X-ray diffraction. These structures are found to be in line with projections based on the chemical and spectroscopic properties, and thus offer an additional confirmation of the proposed reaction mechanisms.
Heterocycles ; Reaction mechanisms ; Schiff bases ; X-Ray structure determination
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Podaci o izdanju
147 (10)
2016.
1825-1837
objavljeno
0026-9247
1434-4475
10.1007/s00706-016-1796-5