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Real-Time In Situ Powder X-ray Diffraction Monitoring of Mechanochemical Synthesis of Pharmaceutical Cocrystals


Halasz, Ivan; Puškarić, Andreas; Kimber, Simon A.J.; Beldon, Patrick J.; Belenguer, Ana M.; Adams, Frank; Honkimäki, Veijo; Dinnebier, Robert E.; Patel, Bhavnita; Jones, William et al.
Real-Time In Situ Powder X-ray Diffraction Monitoring of Mechanochemical Synthesis of Pharmaceutical Cocrystals // Angewandte Chemie. International edition, 52 (2013), 44; 11538-11541. doi:10.1002/anie.201305928 (članak, znanstveni)


Naslov
Real-Time In Situ Powder X-ray Diffraction Monitoring of Mechanochemical Synthesis of Pharmaceutical Cocrystals

Autori
Halasz, Ivan ; Puškarić, Andreas ; Kimber, Simon A.J. ; Beldon, Patrick J. ; Belenguer, Ana M. ; Adams, Frank ; Honkimäki, Veijo ; Dinnebier, Robert E. ; Patel, Bhavnita ; Jones, William ; Štrukil, Vjekoslav ; Friščić, Tomislav

Izvornik
Angewandte Chemie. International edition (1433-7851) 52 (2013), 44; 11538-11541

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Cocrystals; mechanochemistry; pharmaceutical materials; reaction monitoring; X-ray diffraction

Sažetak
We have reported the first real-time, in situ X- ray diffraction study of mechanochemical synthesis and transformations of organic cocrystals. With time resolution in seconds, this technique allows the identification and monitoring of neat and liquid-assisted milling reactions, as well as in situ assessment of changes in the size of crystalline particles.

Projekt / tema
098-0982904-2953 - Studij utjecaja svojstava alumosilikatnih prekursora na njihove transformacije (Josip Bronić)

Izvorni jezik
Engleski

Rad je citiran u bazama podataka
WoSCC, Current Contents, Science Citation Index Expanded Index, Scopus

Znanstvena područja
Kemija