engleski

An Old Story in New Light: X-Ray Powder Diffraction Provides Novel Insights into a Long-Known Organic Solid-State Rearrangement Reaction

The first in situ diffraction study of the long-known solid-state rearrangement of p-bromobenzeneazotribenzoylmethane is reported. This proof-of-principle study demonstrates how modern laboratory X-ray powder diffraction, accompanied by up-to-date processing tools, can be used to monitor and describe mechanisms of organic solid-state reactions while it also underpins its necessity for structural characterisation of in situ formed crystalline phases.

powder diffraction; hot-stage microscopy; solid-state reaction; rearrangement; optical microscopy

nije evidentirano