Napredna pretraga

Pregled bibliografske jedinice broj: 633292

COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL


Ćurković, Lidija; Vugrinčić, Amalija; Siketić, Zdravko; Bačić, Ivana; Levačić, Lidija
COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL // 2nd mediterian conference & new challenges on heat treatment and surface engineering / Smoljan, Božo ; Matijević, Božidar (ur.).
Zagreb: Croatian Society for Heat Treatment and Surface Engineering, 2013. str. 429-434 (poster, međunarodna recenzija, cjeloviti rad (in extenso), znanstveni)


Naslov
COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL

Autori
Ćurković, Lidija ; Vugrinčić, Amalija ; Siketić, Zdravko ; Bačić, Ivana ; Levačić, Lidija

Vrsta, podvrsta i kategorija rada
Radovi u zbornicima skupova, cjeloviti rad (in extenso), znanstveni

Izvornik
2nd mediterian conference & new challenges on heat treatment and surface engineering / Smoljan, Božo ; Matijević, Božidar - Zagreb : Croatian Society for Heat Treatment and Surface Engineering, 2013, 429-434

ISBN
978-953-7690-02-1

Skup
2nd mediterian conference & new challenges on heat treatment and surface engineering

Mjesto i datum
Dubrovnik-Cavtat, Hrvatska, 11-14.06.2013

Vrsta sudjelovanja
Poster

Vrsta recenzije
Međunarodna recenzija

Ključne riječi
Sol-gel; TiO2−ZrO2 films; GD-OES; TOF-ERDA

Sažetak
In this paper, sol-gel TiO2−ZrO2 films with one layer, three layers and five layers were deposited on the X2CrNiMo17-12-2 (AISI 316L) austenitic stainless steel by dip coating method. Calcination was carried out at 400 °C and 600 °C. For quantitative depth profile analysis of sol-gel TiO2−ZrO2 films the following two different analytical techniques were used and compared: glow-discharge optical emission spectrometry (GD-OES) and time-of-flight elastic recoil detection analysis (TOF-ERDA). Obtained results of GD-OES and TOF-ERDA spectrometry indicated that the depth of the deposited films was increased by increasing the number of deposited layers as well as by increasing the calcination temperature. It was found that the thickness of deposited sol-gel TiO2−ZrO2 films varied from 8 to 95 nm, depending on the number of layers and the calcination temperature. Also, it was found that diffusion of some elements (mainly Cr and Fe) from substrate through interface and film was increased by increasing the calcination temperature. Results obtained by GD-OES and TOF-ERDA indicated that both techniques are excellent tools in the field of surface engineering and can be successfully used for determining elemental composition as a function of depth.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Kemijsko inženjerstvo, Strojarstvo



POVEZANOST RADA


Projekt / tema
120-1201833-1789 - Istraživanje strukture i svojstava tehničke keramike i keramičkih prevlaka (Lidija Ćurković, )

Ustanove
Prirodoslovno-matematički fakultet, Zagreb,
Fakultet strojarstva i brodogradnje, Zagreb

Citiraj ovu publikaciju

Ćurković, Lidija; Vugrinčić, Amalija; Siketić, Zdravko; Bačić, Ivana; Levačić, Lidija
COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL // 2nd mediterian conference & new challenges on heat treatment and surface engineering / Smoljan, Božo ; Matijević, Božidar (ur.).
Zagreb: Croatian Society for Heat Treatment and Surface Engineering, 2013. str. 429-434 (poster, međunarodna recenzija, cjeloviti rad (in extenso), znanstveni)
Ćurković, L., Vugrinčić, A., Siketić, Z., Bačić, I. & Levačić, L. (2013) COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL. U: Smoljan, B. & Matijević, B. (ur.)2nd mediterian conference & new challenges on heat treatment and surface engineering.
@article{article, year = {2013}, pages = {429-434}, keywords = {sol-gel, TiO2−ZrO2 films, GD-OES, TOF-ERDA}, isbn = {978-953-7690-02-1}, title = {COMPARISON OF TWO DEPTH PROFILING METHODS FOR ANALYSIS OF SOL-GEL TiO2−ZrO2 FILMS ON STAINLESS STEEL}, keyword = {sol-gel, TiO2−ZrO2 films, GD-OES, TOF-ERDA}, publisher = {Croatian Society for Heat Treatment and Surface Engineering}, publisherplace = {Dubrovnik-Cavtat, Hrvatska} }