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Pregled bibliografske jedinice broj: 600712

Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases

Schilf, Wojciech; Kamieński, Bohdan; Užarević, Krunoslav
Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases // Journal of molecular structure, 1013 (2013), 211-215 doi:10.1016/j.molstruc.2012.10.004 (međunarodna recenzija, članak, znanstveni)

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Naslov
Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases

Autori
Schilf, Wojciech ; Kamieński, Bohdan ; Užarević, Krunoslav

Izvornik
Journal of molecular structure (0022-2860) 1013 (2013); 211-215

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
13C; 15N NMR; CPMAS; tautomerism; hydrogen bond

Sažetak
The five Schiff bases obtained by condensation of dehydroacetic acid, p-phenylenediamine and derivatives of salicylaldehyde were investigated by 13C and 15N CPMAS NMR methods to find the structure of intramolecular hydrogen bridges. Additionally the 15N NMR spectra in CDCl3 were done. The results obtained in the solid state and in solution were compared with the X-ray previously published for some of investigated compounds. The relatively small influence of substituent in salicylaldehyde unit on proton position was found as well as only small difference in the hydrogen bridges structure in both phases, solution and solid state, which is in contrast with results acquired for Schiff bases obtained from simple aliphatic amines.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA

Projekti:
119-1191342-1082 - Novi kompleksni spojevi i materijali-kemijski i biološki katalizatori (Cindrić, Marina, MZOS ) ( CroRIS)

Ustanove:
Prirodoslovno-matematički fakultet, Zagreb

Profili:

Avatar Url Krunoslav Užarević (autor)

Poveznice na cjeloviti tekst rada:

doi www.sciencedirect.com ac.els-cdn.com dx.doi.org

Citiraj ovu publikaciju:

Schilf, Wojciech; Kamieński, Bohdan; Užarević, Krunoslav
Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases // Journal of molecular structure, 1013 (2013), 211-215 doi:10.1016/j.molstruc.2012.10.004 (međunarodna recenzija, članak, znanstveni)
Schilf, W., Kamieński, B. & Užarević, K. (2013) Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases. Journal of molecular structure, 1013, 211-215 doi:10.1016/j.molstruc.2012.10.004.
@article{article, author = {Schilf, Wojciech and Kamie\'{n}ski, Bohdan and U\v{z}arevi\'{c}, Krunoslav}, year = {2013}, pages = {211-215}, DOI = {10.1016/j.molstruc.2012.10.004}, keywords = {13C, 15N NMR, CPMAS, tautomerism, hydrogen bond}, journal = {Journal of molecular structure}, doi = {10.1016/j.molstruc.2012.10.004}, volume = {1013}, issn = {0022-2860}, title = {Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases}, keyword = {13C, 15N NMR, CPMAS, tautomerism, hydrogen bond} }
@article{article, author = {Schilf, Wojciech and Kamie\'{n}ski, Bohdan and U\v{z}arevi\'{c}, Krunoslav}, year = {2013}, pages = {211-215}, DOI = {10.1016/j.molstruc.2012.10.004}, keywords = {13C, 15N NMR, CPMAS, tautomerism, hydrogen bond}, journal = {Journal of molecular structure}, doi = {10.1016/j.molstruc.2012.10.004}, volume = {1013}, issn = {0022-2860}, title = {Nitrogen and carbon CPMAS NMR investigations of keto-enol tautomerism in asymmetric o-hydroxy Schiff bases}, keyword = {13C, 15N NMR, CPMAS, tautomerism, hydrogen bond} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus

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