Mechanosynthesis of nitrosobenzenes: a proof-of-principle study in combining solvent-free synthesis with solvent-free separations (CROSBI ID 184426)
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Podaci o odgovornosti
Huskić, Igor ; Halasz, Ivan ; Friščić, Tomislav ; Vančik, Hrvoj
engleski
Mechanosynthesis of nitrosobenzenes: a proof-of-principle study in combining solvent-free synthesis with solvent-free separations
Mechanochemical Oxone oxidation of selected para-substituted anilines was used as a rapid and solvent-free route to nitrosobenzenes ; besides avoiding bulk solvents and short reaction times, this method exploits high vapour pressures of nitrosobenzenes for the solvent-free separation of the product by sublimation, demonstrating an entirely solvent-free route to chemical synthesis and product isolation.
nitrosobenzenes; mechanochemistry; solvent-free synthesis; sublimation; green chemistry
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