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Synthesis of new steroid-beta-lactam hybrids via palladium-catalyzed aminocarbonylation


Balogh, Janos; Skoda-Foldes, Rita; Vazdar, Katarina; Habuš, Ivan
Synthesis of new steroid-beta-lactam hybrids via palladium-catalyzed aminocarbonylation // Journal of organometallic chemistry, 703 (2012), 51-55 doi:10.1016/j.jorganchem.2011.12.033 (međunarodna recenzija, članak, znanstveni)


Naslov
Synthesis of new steroid-beta-lactam hybrids via palladium-catalyzed aminocarbonylation

Autori
Balogh, Janos ; Skoda-Foldes, Rita ; Vazdar, Katarina ; Habuš, Ivan

Izvornik
Journal of organometallic chemistry (0022-328X) 703 (2012); 51-55

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Beta-lactams ; hybrids ; aminocarbonylation ; palladium ; alkenyl iodides

Sažetak
Steroid-beta-lactam and steroid-beta-lactam-ferrocene conjugates were synthesized via palladium-catalyzed carbonylation of steroidal 17-iodo-16-enes in the presence of 3-amino-azetidin-2-ones. beta-Lactam derivatives have been used for the first time as nucleophyles in the aminocarbonylation reaction. The products were obtained in good yields and were characterized by 1H- and 13C-NMR, IR and HRMS.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekt / tema
098-0982915-2948 - Amino-beta-laktami - intermedijari u sintezi biološki interesantnih spojeva (Vlasta Tomašić, )

Ustanove
Institut "Ruđer Bošković", Zagreb

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus


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