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Feed additives diclazuril and nicarbazin in egg and liver samples from Croatian farms (CROSBI ID 180005)

Prilog u časopisu | izvorni znanstveni rad | međunarodna recenzija

Bilandžić, Nina ; Dolenc, Jožica ; Šinigoj Gačnik, Ksenija ; Varenina, Ivana ; Solomun Kolanović, Božica Feed additives diclazuril and nicarbazin in egg and liver samples from Croatian farms // Food Additives & Contaminants Part B-Surveillance, 6 (2013), 2; 90-97. doi: 10.1080/19393210.2012.727474

Podaci o odgovornosti

Bilandžić, Nina ; Dolenc, Jožica ; Šinigoj Gačnik, Ksenija ; Varenina, Ivana ; Solomun Kolanović, Božica

engleski

Feed additives diclazuril and nicarbazin in egg and liver samples from Croatian farms

A total of 307 egg and 275 liver samples were examined for nicarbazin and 365 eggs for diclazuril over a 30 month period. Enzyme-linked immunosorbent assay methods (ELISA) used for quantification were validated according to the guidelines laid down by European Commission Decision 2002/657/EC. Non- compliant samples of egg and liver determined by ELISA were subjected to confirmation by the LC-MS/MS method. Mean diclazuril concentrations obtained in egg samples were 0.31 μg kg-1, i.e. below the MRL level. A concentration of 2.26 μg kg-1 was determined by ELISA in only one egg sample, though confirmation by LC-MS/MS gave a value of 1.6 μg kg-1. Mean nicarbazin levels determined were 1.85 μg kg-1 in egg and 21.1 μg kg-1 in liver samples. Four samples, one egg and three liver, yielded elevated concentrations of nicarbazin. Only in the egg sample LC-MS/MS method confirmed nicarbazin above the MRL value (106 μg kg- 1).

diclazuril ; nicarbazin ; egg ; liver ; EIA ; LC-MS/MS

nije evidentirano

nije evidentirano

nije evidentirano

nije evidentirano

nije evidentirano

nije evidentirano

Podaci o izdanju

6 (2)

2013.

90-97

objavljeno

1939-3210

1939-3229

10.1080/19393210.2012.727474

Povezanost rada

Javno zdravstvo i zdravstvena zaštita, Veterinarska medicina

Poveznice
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