A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation (CROSBI ID 169252)
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Podaci o odgovornosti
Atkinson, Manza B.J. ; Halasz, Ivan ; Bučar, Dejan-Krešimir ; Dinnebier, Robert E. ; Mariappan, Santhana S. V. ; Sokolov, Anatoliy N. ; MacGillivray, Leonard R.
engleski
A solid-state trimerisation of a diene diacid affords a bicyclobutyl: reactant structure from X-ray powder data and product separation and structure determination via co-crystallisation
A bicyclobutyl that bears six carboxylic acid groups results from a trimerisation of a diene diacid in the solid state. Powder X-ray diffraction and a co-crystallisation are used to solve the structure of the diene and elucidate the stereochemistry of the bicyclobutyl, respectively.
cocrystal; solid-state reaction; photodimerisation; diffraction; crystal structure
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