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Pregled bibliografske jedinice broj: 368356

Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines – Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone


Gazivoda, Tatjana; Raić-Malić, Silvana; Hergold-Brundić; Antonija; Cetina, Mario
Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines – Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone // Molecules, 13 (2008), 11; 2786-2795 (međunarodna recenzija, članak, znanstveni)


CROSBI ID: 368356 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines – Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone

Autori
Gazivoda, Tatjana ; Raić-Malić, Silvana ; Hergold-Brundić ; Antonija ; Cetina, Mario

Izvornik
Molecules (1420-3049) 13 (2008), 11; 2786-2795

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
5-(2-Haloethyl)Pyrimidine; Synthesis; X-ray crystal structure; Hydrogen bonds

Sažetak
Three novel 5-(2-haloethyl)pyrimidine derivatives were synthesized and characterized by 1H-NMR, 13C-NMR, MS, IR spectra and elemental analysis. Iodine and chlorine atoms in the C-5 side chain were introduced by reaction of 5-(2-hydroxyethyl)pyrimidine with hydroiodic acid and phosphoryl chloride, respectively. The structure of the intermediate  -(1-carbamyliminomethylene)- -butyrolactone was determined by X-ray crystal structure analysis. The molecule deviates very slightly from planarity. Three N H• • • O hydrogen bonds link the molecules into one-dimensional chains of edge-fused rings.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekti:
125-0982464-2925 - Razvoj i primjena novih molekula u pozitron-emisijskoj tomografiji (PET) (Raić-Malić, Silvana, MZOS ) ( POIROT)

Ustanove:
Tekstilno-tehnološki fakultet, Zagreb,
Prirodoslovno-matematički fakultet, Zagreb,
Fakultet kemijskog inženjerstva i tehnologije, Zagreb


Citiraj ovu publikaciju:

Gazivoda, Tatjana; Raić-Malić, Silvana; Hergold-Brundić; Antonija; Cetina, Mario
Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines – Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone // Molecules, 13 (2008), 11; 2786-2795 (međunarodna recenzija, članak, znanstveni)
Gazivoda, T., Raić-Malić, S., Hergold-Brundić, Antonija & Cetina, M. (2008) Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines – Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone. Molecules, 13 (11), 2786-2795.
@article{article, year = {2008}, pages = {2786-2795}, keywords = {5-(2-Haloethyl)Pyrimidine, Synthesis, X-ray crystal structure, Hydrogen bonds}, journal = {Molecules}, volume = {13}, number = {11}, issn = {1420-3049}, title = {Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines and \#8211; Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone}, keyword = {5-(2-Haloethyl)Pyrimidine, Synthesis, X-ray crystal structure, Hydrogen bonds} }
@article{article, year = {2008}, pages = {2786-2795}, keywords = {5-(2-Haloethyl)Pyrimidine, Synthesis, X-ray crystal structure, Hydrogen bonds}, journal = {Molecules}, volume = {13}, number = {11}, issn = {1420-3049}, title = {Synthesis and Structural Characterization of the 5-(2-Haloethyl)Pyrimidines and \#8211; Hydrogen-Bonded chains in alpha-(1-Carbamyliminomethylene)-gama-Butyrolactone}, keyword = {5-(2-Haloethyl)Pyrimidine, Synthesis, X-ray crystal structure, Hydrogen bonds} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE





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