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Pregled bibliografske jedinice broj: 287857

Performance of New HPLC Chiral Stationary Phase Derived from N-(3, 5-dinitrobenzoyl)-D-alpha-Phenylglycine with Quinoxaline Branching Unit


Moslavac Forjan, Davorka; Vinković, Vladimir; Kontrec, Darko
Performance of New HPLC Chiral Stationary Phase Derived from N-(3, 5-dinitrobenzoyl)-D-alpha-Phenylglycine with Quinoxaline Branching Unit // Acta Chromatographica, 17 (2006), 97-107 (međunarodna recenzija, članak, znanstveni)


Naslov
Performance of New HPLC Chiral Stationary Phase Derived from N-(3, 5-dinitrobenzoyl)-D-alpha-Phenylglycine with Quinoxaline Branching Unit

Autori
Moslavac Forjan, Davorka ; Vinković, Vladimir ; Kontrec, Darko

Izvornik
Acta Chromatographica (1233-2356) 17 (2006); 97-107

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Chiral stationary phases; enantioseparation

Sažetak
New brush-type HPLC chiral stationary phase (CSP-1) comprising pi-acidic N-(3, 5-dinitrobenzoyl)-D-alpha-phenylglycine chiral unit bound to quinoxaline unit of the modified  -aminopropyl silica gel via 1, 2-diaminoethane spacer was prepared by solid-phase synthesis. The column packed with CSP-1 was tested for the separation of racemates TR-1 TR-22 with various functional groups and the results are compared with those obtained by using three structurally related chiral stationary phases CSP-2 CSP-4.

Izvorni jezik
Engleski

Znanstvena područja
Kemija



POVEZANOST RADA


Projekt / tema
0098051

Ustanove
Institut "Ruđer Bošković", Zagreb

Časopis indeksira:


  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus