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Microwave irradiation applied with success to cycloaddition reaction of N-Propargyl-N-p-tolyl-N-2-furfurylamines (CROSBI ID 501771)

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Mance, Ana Dunja ; Jakopčić, Krešimir Microwave irradiation applied with success to cycloaddition reaction of N-Propargyl-N-p-tolyl-N-2-furfurylamines // Conference, Workshop and Exibition on Microwave Chemistry : MAOS 2004 Graz, Austrija, 20.09.2004-21.09.2004

Podaci o odgovornosti

Mance, Ana Dunja ; Jakopčić, Krešimir

engleski

Microwave irradiation applied with success to cycloaddition reaction of N-Propargyl-N-p-tolyl-N-2-furfurylamines

The new N-(5-substituted.2-furfuryl)-N-prop-2-ynyl-p-toluidines were prepared according to the reported procedure and intramolecular Diels-Alder reaction was performed by heating a benzene solution of the amines under nitrogen for three days.The intramolecular Diels-Alder reaction of the 5-H and 5-CH3 substituted amines was also performed under microwave irradiation conditions giving the cycloaddition products 5-H and 5-CH3 substituted N-p-tolyl-5-methyl-5, 7a-dihydro-5, 7a-epoxyisoindolines. Comparing the results of the usual thermal and the MAOS reaction, we confirmed our expectations that MAOS could promote the outcome of IMDA reaction of the suitably N-substituted tertiary 2-furfuryl-amines.

MAOS; IMDAF; epoxyisoindoline; [4+2]cycloaddition; alkynylarylfurfurylamine

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Podaci o prilogu

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Podaci o skupu

Conference, Workshop and Exibition on Microwave Chemistry : MAOS 2004

poster

20.09.2004-21.09.2004

Graz, Austrija

Povezanost rada

Kemijsko inženjerstvo