Pretražite po imenu i prezimenu autora, mentora, urednika, prevoditelja

Napredna pretraga

Pregled bibliografske jedinice broj: 1157374

Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography


Jurin, Mladenka; Kontrec, Darko; Dražić, Tonko; Roje, Marin
Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography // Croatica chemica acta, 93 (2020), 3; 203-213 doi:10.5562/cca3781 (međunarodna recenzija, članak, znanstveni)


CROSBI ID: 1157374 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography

Autori
Jurin, Mladenka ; Kontrec, Darko ; Dražić, Tonko ; Roje, Marin

Izvornik
Croatica chemica acta (0011-1643) 93 (2020), 3; 203-213

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
β-lactam ureas ; enantioseparation ; SFC chromatography ; chiral stationary phases (CSP's)

Sažetak
In this study the enantioseparation of (±)-trans-β-lactam ureas 1a–g by supercritical fluid chromatography (SFC) was examined using different polysaccharide based chiral stationary phases (CSPs), and CO2/alcohol (70:30, V/V) as the mobile phase. The influence of CSP type (coated or immobilized), modifiers (alcohols), additive (isopropylamine), temperature and backpressure on enantioseparation were examined. From five tested columns, only the column filled with tris-(4-methylphenylcarbamoyl) cellulose selector proved superior in terms of broad range substrate acceptability and selectivity.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Interdisciplinarne prirodne znanosti, Kemijsko inženjerstvo



POVEZANOST RADA


Projekti:
EK-KF-KK.01.1.1.01.0002 - Bioprospecting Jadranskog mora (Čož-Rakovac, Rozelinda; Dragović-Uzelac, Verica; Šantek, Božidar; Jokić, Stela; Jerković, Igor; Kraljević Pavelić, Sandra, EK - KK.01.1.1.01) ( POIROT)
MZOS-N/A - Znanstveni centar izvrsnosti za bioprospecting mora (BioProCro) (Čož-Rakovac, Rozelinda; Roje, Marin, MZOS ) ( POIROT)

Ustanove:
Institut "Ruđer Bošković", Zagreb

Profili:

Avatar Url Marin Roje (autor)

Avatar Url Darko Kontrec (autor)

Avatar Url Mladenka Jurin (autor)

Poveznice na cjeloviti tekst rada:

doi doi.org hrcak.srce.hr fulir.irb.hr

Citiraj ovu publikaciju:

Jurin, Mladenka; Kontrec, Darko; Dražić, Tonko; Roje, Marin
Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography // Croatica chemica acta, 93 (2020), 3; 203-213 doi:10.5562/cca3781 (međunarodna recenzija, članak, znanstveni)
Jurin, M., Kontrec, D., Dražić, T. & Roje, M. (2020) Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography. Croatica chemica acta, 93 (3), 203-213 doi:10.5562/cca3781.
@article{article, author = {Jurin, Mladenka and Kontrec, Darko and Dra\v{z}i\'{c}, Tonko and Roje, Marin}, year = {2020}, pages = {203-213}, DOI = {10.5562/cca3781}, keywords = {β-lactam ureas, enantioseparation, SFC chromatography, chiral stationary phases (CSP's)}, journal = {Croatica chemica acta}, doi = {10.5562/cca3781}, volume = {93}, number = {3}, issn = {0011-1643}, title = {Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography}, keyword = {β-lactam ureas, enantioseparation, SFC chromatography, chiral stationary phases (CSP's)} }
@article{article, author = {Jurin, Mladenka and Kontrec, Darko and Dra\v{z}i\'{c}, Tonko and Roje, Marin}, year = {2020}, pages = {203-213}, DOI = {10.5562/cca3781}, keywords = {β-lactam ureas, enantioseparation, SFC chromatography, chiral stationary phases (CSP's)}, journal = {Croatica chemica acta}, doi = {10.5562/cca3781}, volume = {93}, number = {3}, issn = {0011-1643}, title = {Enantioseparation of (±)-trans-β-lactam Ureas by Supercritical Fluid Chromatography}, keyword = {β-lactam ureas, enantioseparation, SFC chromatography, chiral stationary phases (CSP's)} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus


Citati:





    Contrast
    Increase Font
    Decrease Font
    Dyslexic Font