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Pregled bibliografske jedinice broj: 1139409

Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate


Šafranko, Silvija; Goman, Sara; Goman, Dominik; Jokić, Stela; Delač Marion, Ida; Matijaković Mlinarić, Nives; Selmani, Atiđa; Medvidović‑Kosanović, Martina; Stanković, Anamarija
Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate // Crystals, 11 (2021), 8; 954, 16 doi:10.3390/cryst11080954 (međunarodna recenzija, članak, znanstveni)


CROSBI ID: 1139409 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate

Autori
Šafranko, Silvija ; Goman, Sara ; Goman, Dominik ; Jokić, Stela ; Delač Marion, Ida ; Matijaković Mlinarić, Nives ; Selmani, Atiđa ; Medvidović‑Kosanović, Martina ; Stanković, Anamarija

Izvornik
Crystals (2073-4352) 11 (2021), 8; 954, 16

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
calcium oxalate monohydrate ; calcium oxalate dihydrate ; response surface methodology ; pathological biomineralization ; gallic acid

Sažetak
The search for an efficient drug or inhibitor in the formation process of kidney stones has been a promising research topic towards reducing the risks of the formation of disease. However, several challenges have been faced in investigating the most common constituents of kidney stones, calcium oxalate and its hydrate forms (COM, COD and COT). This study focuses on the preparation and structural characterization (TG, XRD, FTIR, SEM) of calcium oxalate hydrates in the presence of gallic acid (GA) and by varying operating parameters such as temperature (25 °C, 36.5 °C and 48 °C), pH (5.6, 6.5 and 7.5) and amount of added GA (ranging from 100 mg to 1000 mg). Response surface methodology was applied in order to evaluate the effects of operating parameters in the formation of COM and COD, and for the process optimization towards maximizing their content in samples. The results indicated that GA inhibited the formation of COM (0–100%) and promoted the formation of COD (0 ≤ 99%), while a medium pH and the amount of added GA showed a significant effect in the process of COD formation. In order to investigate the interactions established in the formation process and the possible adsorption between GA and the formed crystals, electrochemical measurements were performed.

Izvorni jezik
Engleski

Znanstvena područja
Kemija, Interdisciplinarne prirodne znanosti, Prehrambena tehnologija



POVEZANOST RADA


Projekti:
EK-EFRR-KK.01.1.1.01.0001 - Potpora vrhunskim istraživanjima Centra izvrsnosti za napredne materijale i senzore (Ivanda, Mile; Jakšić, Milko; Stipčević, Mario; Kralj, Marko, EK - KK.01.1.1.01) ( POIROT)

Ustanove:
Institut za fiziku, Zagreb,
Institut "Ruđer Bošković", Zagreb,
Prehrambeno-tehnološki fakultet, Osijek,
Sveučilište u Osijeku - Odjel za kemiju

Poveznice na cjeloviti tekst rada:

doi www.mdpi.com fulir.irb.hr

Citiraj ovu publikaciju:

Šafranko, Silvija; Goman, Sara; Goman, Dominik; Jokić, Stela; Delač Marion, Ida; Matijaković Mlinarić, Nives; Selmani, Atiđa; Medvidović‑Kosanović, Martina; Stanković, Anamarija
Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate // Crystals, 11 (2021), 8; 954, 16 doi:10.3390/cryst11080954 (međunarodna recenzija, članak, znanstveni)
Šafranko, S., Goman, S., Goman, D., Jokić, S., Delač Marion, I., Matijaković Mlinarić, N., Selmani, A., Medvidović‑Kosanović, M. & Stanković, A. (2021) Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate. Crystals, 11 (8), 954, 16 doi:10.3390/cryst11080954.
@article{article, author = {\v{S}afranko, Silvija and Goman, Sara and Goman, Dominik and Joki\'{c}, Stela and Dela\v{c} Marion, Ida and Matijakovi\'{c} Mlinari\'{c}, Nives and Selmani, Ati\dja and Medvidovi\'{c}‑Kosanovi\'{c}, Martina and Stankovi\'{c}, Anamarija}, year = {2021}, pages = {16}, DOI = {10.3390/cryst11080954}, chapter = {954}, keywords = {calcium oxalate monohydrate, calcium oxalate dihydrate, response surface methodology, pathological biomineralization, gallic acid}, journal = {Crystals}, doi = {10.3390/cryst11080954}, volume = {11}, number = {8}, issn = {2073-4352}, title = {Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate}, keyword = {calcium oxalate monohydrate, calcium oxalate dihydrate, response surface methodology, pathological biomineralization, gallic acid}, chapternumber = {954} }
@article{article, author = {\v{S}afranko, Silvija and Goman, Sara and Goman, Dominik and Joki\'{c}, Stela and Dela\v{c} Marion, Ida and Matijakovi\'{c} Mlinari\'{c}, Nives and Selmani, Ati\dja and Medvidovi\'{c}‑Kosanovi\'{c}, Martina and Stankovi\'{c}, Anamarija}, year = {2021}, pages = {16}, DOI = {10.3390/cryst11080954}, chapter = {954}, keywords = {calcium oxalate monohydrate, calcium oxalate dihydrate, response surface methodology, pathological biomineralization, gallic acid}, journal = {Crystals}, doi = {10.3390/cryst11080954}, volume = {11}, number = {8}, issn = {2073-4352}, title = {Calcium oxalate and gallic acid: structural characterization and process optimization toward obtaining high contents of calcium oxalate monohydrate and dihydrate}, keyword = {calcium oxalate monohydrate, calcium oxalate dihydrate, response surface methodology, pathological biomineralization, gallic acid}, chapternumber = {954} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus


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