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Pregled bibliografske jedinice broj: 1059454

Direct Visualization of a Mechanochemically Induced Molecular Rearrangement


Ardila-Fierro, Karen J.; Lukin, Stipe; Etter, Martin; Užarević, Krunoslav; Halasz, Ivan; Bolm, Carsten; Hernández, José G.
Direct Visualization of a Mechanochemically Induced Molecular Rearrangement // Angewandte Chemie. International edition, 59 (2020), 32; 13458, 13462 doi:10.1002/anie.201914921 (međunarodna recenzija, članak, znanstveni)


CROSBI ID: 1059454 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Direct Visualization of a Mechanochemically Induced Molecular Rearrangement
(Direct Visualization of a Mechanochemically Induced Molecular Rearrangemen)

Autori
Ardila-Fierro, Karen J. ; Lukin, Stipe ; Etter, Martin ; Užarević, Krunoslav ; Halasz, Ivan ; Bolm, Carsten ; Hernández, José G.

Izvornik
Angewandte Chemie. International edition (1433-7851) 59 (2020), 32; 13458, 13462

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Mechanochemistry ; Mechanochemical synthesis ; Organic synthesis ; Molecular rearrangement ; In situ monitoring ; Raman spectroscopy ; Synchrotron diffraction

Sažetak
Recent progress in the field of mechanochemistry has expanded the discovery of mechanically induced chemical transformations to several areas of science. However, a general fundamental understanding of how mechanochemical reactions by ball milling occur has remained unreached. For this, we have now implemented in‐situ monitoring of a mechanochemically induced molecular rearrangement by synchrotron X‐ray powder diffraction, Raman spectroscopy, and real‐time temperature sensing. The results of this study demonstrate that molecular rearrangements can be accomplished in the solid- state by ball milling, and how in‐situ monitoring techniques enable the visualization of the changes occurring at the exact instant of a molecular migration. In this study, during the mechanochemical benzil‐benzilic acid rearrangement.

Izvorni jezik
Engleski

Znanstvena područja
Kemija

Napomena
Communication



POVEZANOST RADA


Projekti:
PZS-2019-02-4129

Ustanove:
Institut "Ruđer Bošković", Zagreb

Profili:

Avatar Url Ivan Halasz (autor)

Avatar Url Stipe Lukin (autor)

Avatar Url Krunoslav Užarević (autor)

Citiraj ovu publikaciju

Ardila-Fierro, Karen J.; Lukin, Stipe; Etter, Martin; Užarević, Krunoslav; Halasz, Ivan; Bolm, Carsten; Hernández, José G.
Direct Visualization of a Mechanochemically Induced Molecular Rearrangement // Angewandte Chemie. International edition, 59 (2020), 32; 13458, 13462 doi:10.1002/anie.201914921 (međunarodna recenzija, članak, znanstveni)
Ardila-Fierro, K., Lukin, S., Etter, M., Užarević, K., Halasz, I., Bolm, C. & Hernández, J. (2020) Direct Visualization of a Mechanochemically Induced Molecular Rearrangement. Angewandte Chemie. International edition, 59 (32), 13458, 13462 doi:10.1002/anie.201914921.
@article{article, year = {2020}, pages = {13462}, DOI = {10.1002/anie.201914921}, chapter = {13458}, keywords = {Mechanochemistry, Mechanochemical synthesis, Organic synthesis, Molecular rearrangement, In situ monitoring, Raman spectroscopy, Synchrotron diffraction}, journal = {Angewandte Chemie. International edition}, doi = {10.1002/anie.201914921}, volume = {59}, number = {32}, issn = {1433-7851}, title = {Direct Visualization of a Mechanochemically Induced Molecular Rearrangement}, keyword = {Mechanochemistry, Mechanochemical synthesis, Organic synthesis, Molecular rearrangement, In situ monitoring, Raman spectroscopy, Synchrotron diffraction}, chapternumber = {13458} }
@article{article, year = {2020}, pages = {13462}, DOI = {10.1002/anie.201914921}, chapter = {13458}, keywords = {Mechanochemistry, Mechanochemical synthesis, Organic synthesis, Molecular rearrangement, In situ monitoring, Raman spectroscopy, Synchrotron diffraction}, journal = {Angewandte Chemie. International edition}, doi = {10.1002/anie.201914921}, volume = {59}, number = {32}, issn = {1433-7851}, title = {Direct Visualization of a Mechanochemically Induced Molecular Rearrangemen}, keyword = {Mechanochemistry, Mechanochemical synthesis, Organic synthesis, Molecular rearrangement, In situ monitoring, Raman spectroscopy, Synchrotron diffraction}, chapternumber = {13458} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus
  • MEDLINE


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