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Pregled bibliografske jedinice broj: 1045579

Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry


Mornar, Ana; Buhač, Tajana; Amidžić Klarić, Daniela; Klarić, Ilija; Sertić, Miranda; Nigović, Biljana
Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry // Food Analytical Methods, 13 (2020), 2; 482-495 doi:10.1007/s12161-019-01653-x (međunarodna recenzija, članak, znanstveni)


CROSBI ID: 1045579 Za ispravke kontaktirajte CROSBI podršku putem web obrasca

Naslov
Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry

Autori
Mornar, Ana ; Buhač, Tajana ; Amidžić Klarić, Daniela ; Klarić, Ilija ; Sertić, Miranda ; Nigović, Biljana

Izvornik
Food Analytical Methods (1936-9751) 13 (2020), 2; 482-495

Vrsta, podvrsta i kategorija rada
Radovi u časopisima, članak, znanstveni

Ključne riječi
Phytoestrogens ; Multi-target analysis ; Liquid chromatography tandem mass spectrometry ; Dietary supplements

Sažetak
This work was carried out to develop a high- performance liquid chromatography tandem mass spectrometry method for simultaneous determination of 11 marker compounds in phytoestrogen-rich food and dietary supplements (raw materials and formulated products) prepared from various sources: soy, red clover, chastetree, hop, and flax. The method was fully validated and showed detection limits varying from 0.2 to 1.5 μg/mL, average recoveries ranging from 95 to 105%, and relative standard deviation values lower than 4.98%. Evidently lower amounts of phytoestrogens were found in food samples than in the dietary supplements. Calculations for the actual daily dose of total phytoestrogens ranged from 0.01 to 6.61 mg among the different products. All derived total phytoestrogen amounts turned out to be below the total content stated by manufacturers (less than 63% of the claimed specifications). Moreover, two samples did not contained phytoestrogens at all. The most eye-catching batch-tobatch deviations were represented by chasteberry-based products (relative standard deviation higher than 9.8%).

Izvorni jezik
Engleski

Znanstvena područja
Farmacija



POVEZANOST RADA


Ustanove
Farmaceutsko-biokemijski fakultet, Zagreb

Citiraj ovu publikaciju

Mornar, Ana; Buhač, Tajana; Amidžić Klarić, Daniela; Klarić, Ilija; Sertić, Miranda; Nigović, Biljana
Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry // Food Analytical Methods, 13 (2020), 2; 482-495 doi:10.1007/s12161-019-01653-x (međunarodna recenzija, članak, znanstveni)
Mornar, A., Buhač, T., Amidžić Klarić, D., Klarić, I., Sertić, M. & Nigović, B. (2020) Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry. Food Analytical Methods, 13 (2), 482-495 doi:10.1007/s12161-019-01653-x.
@article{article, year = {2020}, pages = {482-495}, DOI = {DOI 10.1007/s12161-019-01653-x}, keywords = {Phytoestrogens, Multi-target analysis, Liquid chromatography tandem mass spectrometry, Dietary supplements}, journal = {Food Analytical Methods}, doi = {DOI 10.1007/s12161-019-01653-x}, volume = {13}, number = {2}, issn = {1936-9751}, title = {Multi-targeted Screening of Phytoestrogens in Food, Raw Material, and Dietary Supplements by Liquid Chromatography with Tandem Mass Spectrometry}, keyword = {Phytoestrogens, Multi-target analysis, Liquid chromatography tandem mass spectrometry, Dietary supplements} }

Časopis indeksira:


  • Current Contents Connect (CCC)
  • Web of Science Core Collection (WoSCC)
    • Science Citation Index Expanded (SCI-EXP)
    • SCI-EXP, SSCI i/ili A&HCI
  • Scopus


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